High Field Solid-State NMR Spectroscopy Investigation of 15N‑Labeled Rosette Nanotubes: Hydrogen Bond Network and Channel-Bound Water

15N-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water mol...

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Bibliographic Details
Published in:Journal of the American Chemical Society 2016-05, Vol.138 (19), p.6115-6118
Main Authors: Fenniri, Hicham, Tikhomirov, Grigory A, Brouwer, Darren H, Bouatra, Souhaila, El Bakkari, Mounir, Yan, Zhimin, Cho, Jae-Young, Yamazaki, Takeshi
Format: Article
Language:English
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Summary:15N-labeled rosette nanotubes were synthesized and investigated using high-field solid-state NMR spectroscopy, X-ray diffraction, atomic force microscopy, and electron microscopy. The results established the H-bond network involved in the self-assembly of the nanostructure as well as bound water molecules in the nanotube’s channel.
ISSN:0002-7863
1520-5126
DOI:10.1021/jacs.6b02420