Loading…

The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition

Scanning electron microscopy combined with energy dispersive X-ray analysis (SEM/EDX) was used to identify the gunshot residue (GSR) particles discharged by lead-free Sintox ammunition. Sintox GSR particles are characterized by spheroidal particles mainly consisting of titanium (Ti) and zinc (Zn). T...

Full description

Saved in:
Bibliographic Details
Published in:Journal of forensic sciences 1994-03, Vol.39 (2), p.532-536
Main Authors: Gunaratnam, L, Himberg, K
Format: Article
Language:English
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
cited_by cdi_FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83
cites cdi_FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83
container_end_page 536
container_issue 2
container_start_page 532
container_title Journal of forensic sciences
container_volume 39
creator Gunaratnam, L
Himberg, K
description Scanning electron microscopy combined with energy dispersive X-ray analysis (SEM/EDX) was used to identify the gunshot residue (GSR) particles discharged by lead-free Sintox ammunition. Sintox GSR particles are characterized by spheroidal particles mainly consisting of titanium (Ti) and zinc (Zn). The results obtained in this study are in agreement with the hypothesis that GSR particles are formed by rapid condensation and solidification of vaporized and molten primer and bullet materials as a result of sudden temperature quench. The surface morphology of Ti-Zn particles is an essential criterion for their identification as gunshot residue particles and for discrimination against Ti-Zn environmental particles.
doi_str_mv 10.1520/JFS13626J
format article
fullrecord <record><control><sourceid>proquest_astm_</sourceid><recordid>TN_cdi_astm_journals_10_1520_JFS13626J</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1308646627</sourcerecordid><originalsourceid>FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83</originalsourceid><addsrcrecordid>eNpt0MtKAzEUBuAgCtbqwjcICIKL0VxmMpNlKba2FCy2rkMmF5rSmdQkA-rTO6Uigq7OWXz_f-AAcI3RPS4IephPVpgywuYnYICLgmU5IvwUDBAiJMOYV-fgIsYtQohhhgdgud4YONOmTc46JZPzLfQWTrs2bnyCLyY63Rm4lCE5tTMR2uAbuDBSZ5NgDFy5Nvl3OGqarnWH9CU4s3IXzdX3HILXyeN6_JQtnqez8WiRSUrzlOUVKbSmrLKaccIR7Vdem9pKZStN65IbpRDBxmAiLa4rzcsSa1vUVKnSVnQIbo69--DfOhOT2PoutP1JgSmqWM4YKXt1d1Qq-BiDsWIfXCPDh8BIHB4mfh7W29ujlTE1v9r-geV_sAeCckHEp9v_TYm9tvQLM617ew</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1308646627</pqid></control><display><type>article</type><title>The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition</title><source>ASTM Journals</source><creator>Gunaratnam, L ; Himberg, K</creator><creatorcontrib>Gunaratnam, L ; Himberg, K</creatorcontrib><description>Scanning electron microscopy combined with energy dispersive X-ray analysis (SEM/EDX) was used to identify the gunshot residue (GSR) particles discharged by lead-free Sintox ammunition. Sintox GSR particles are characterized by spheroidal particles mainly consisting of titanium (Ti) and zinc (Zn). The results obtained in this study are in agreement with the hypothesis that GSR particles are formed by rapid condensation and solidification of vaporized and molten primer and bullet materials as a result of sudden temperature quench. The surface morphology of Ti-Zn particles is an essential criterion for their identification as gunshot residue particles and for discrimination against Ti-Zn environmental particles.</description><identifier>ISSN: 0022-1198</identifier><identifier>EISSN: 1556-4029</identifier><identifier>DOI: 10.1520/JFS13626J</identifier><identifier>CODEN: JFSCAS</identifier><language>eng</language><publisher>Mundelein, Ill: Callaghan and Co</publisher><ispartof>Journal of forensic sciences, 1994-03, Vol.39 (2), p.532-536</ispartof><rights>All rights reserved. This material may not be reproduced or copied, in whole or in part, in any printed, mechanical, electronic, film, or other distribution and storage media, without the written consent of the publisher.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83</citedby><cites>FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,9791,27924,27925</link.rule.ids></links><search><creatorcontrib>Gunaratnam, L</creatorcontrib><creatorcontrib>Himberg, K</creatorcontrib><title>The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition</title><title>Journal of forensic sciences</title><description>Scanning electron microscopy combined with energy dispersive X-ray analysis (SEM/EDX) was used to identify the gunshot residue (GSR) particles discharged by lead-free Sintox ammunition. Sintox GSR particles are characterized by spheroidal particles mainly consisting of titanium (Ti) and zinc (Zn). The results obtained in this study are in agreement with the hypothesis that GSR particles are formed by rapid condensation and solidification of vaporized and molten primer and bullet materials as a result of sudden temperature quench. The surface morphology of Ti-Zn particles is an essential criterion for their identification as gunshot residue particles and for discrimination against Ti-Zn environmental particles.</description><issn>0022-1198</issn><issn>1556-4029</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1994</creationdate><recordtype>article</recordtype><recordid>eNpt0MtKAzEUBuAgCtbqwjcICIKL0VxmMpNlKba2FCy2rkMmF5rSmdQkA-rTO6Uigq7OWXz_f-AAcI3RPS4IephPVpgywuYnYICLgmU5IvwUDBAiJMOYV-fgIsYtQohhhgdgud4YONOmTc46JZPzLfQWTrs2bnyCLyY63Rm4lCE5tTMR2uAbuDBSZ5NgDFy5Nvl3OGqarnWH9CU4s3IXzdX3HILXyeN6_JQtnqez8WiRSUrzlOUVKbSmrLKaccIR7Vdem9pKZStN65IbpRDBxmAiLa4rzcsSa1vUVKnSVnQIbo69--DfOhOT2PoutP1JgSmqWM4YKXt1d1Qq-BiDsWIfXCPDh8BIHB4mfh7W29ujlTE1v9r-geV_sAeCckHEp9v_TYm9tvQLM617ew</recordid><startdate>19940301</startdate><enddate>19940301</enddate><creator>Gunaratnam, L</creator><creator>Himberg, K</creator><general>Callaghan and Co</general><scope>AAYXX</scope><scope>CITATION</scope><scope>IOIBA</scope><scope>K30</scope><scope>PAAUG</scope><scope>PAWHS</scope><scope>PAWZZ</scope><scope>PAXOH</scope><scope>PBHAV</scope><scope>PBQSW</scope><scope>PBYQZ</scope><scope>PCIWU</scope><scope>PCMID</scope><scope>PCZJX</scope><scope>PDGRG</scope><scope>PDWWI</scope><scope>PETMR</scope><scope>PFVGT</scope><scope>PGXDX</scope><scope>PIHIL</scope><scope>PISVA</scope><scope>PJCTQ</scope><scope>PJTMS</scope><scope>PLCHJ</scope><scope>PMHAD</scope><scope>PNQDJ</scope><scope>POUND</scope><scope>PPLAD</scope><scope>PQAPC</scope><scope>PQCAN</scope><scope>PQCMW</scope><scope>PQEME</scope><scope>PQHKH</scope><scope>PQMID</scope><scope>PQNCT</scope><scope>PQNET</scope><scope>PQSCT</scope><scope>PQSET</scope><scope>PSVJG</scope><scope>PVMQY</scope><scope>PZGFC</scope></search><sort><creationdate>19940301</creationdate><title>The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition</title><author>Gunaratnam, L ; Himberg, K</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1994</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gunaratnam, L</creatorcontrib><creatorcontrib>Himberg, K</creatorcontrib><collection>CrossRef</collection><collection>Periodicals Index Online Segment 29</collection><collection>Periodicals Index Online</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - West</collection><collection>Primary Sources Access (Plan D) - International</collection><collection>Primary Sources Access &amp; Build (Plan A) - MEA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Midwest</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Northeast</collection><collection>Primary Sources Access (Plan D) - Southeast</collection><collection>Primary Sources Access (Plan D) - North Central</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Southeast</collection><collection>Primary Sources Access (Plan D) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - UK / I</collection><collection>Primary Sources Access (Plan D) - Canada</collection><collection>Primary Sources Access (Plan D) - EMEALA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - North Central</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - International</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - International</collection><collection>Primary Sources Access (Plan D) - West</collection><collection>Periodicals Index Online Segments 1-50</collection><collection>Primary Sources Access (Plan D) - APAC</collection><collection>Primary Sources Access (Plan D) - Midwest</collection><collection>Primary Sources Access (Plan D) - MEA</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - Canada</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - UK / I</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - EMEALA</collection><collection>Primary Sources Access &amp; Build (Plan A) - APAC</collection><collection>Primary Sources Access &amp; Build (Plan A) - Canada</collection><collection>Primary Sources Access &amp; Build (Plan A) - West</collection><collection>Primary Sources Access &amp; Build (Plan A) - EMEALA</collection><collection>Primary Sources Access (Plan D) - Northeast</collection><collection>Primary Sources Access &amp; Build (Plan A) - Midwest</collection><collection>Primary Sources Access &amp; Build (Plan A) - North Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - Northeast</collection><collection>Primary Sources Access &amp; Build (Plan A) - South Central</collection><collection>Primary Sources Access &amp; Build (Plan A) - Southeast</collection><collection>Primary Sources Access (Plan D) - UK / I</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - APAC</collection><collection>Primary Sources Access—Foundation Edition (Plan E) - MEA</collection><jtitle>Journal of forensic sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gunaratnam, L</au><au>Himberg, K</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition</atitle><jtitle>Journal of forensic sciences</jtitle><date>1994-03-01</date><risdate>1994</risdate><volume>39</volume><issue>2</issue><spage>532</spage><epage>536</epage><pages>532-536</pages><issn>0022-1198</issn><eissn>1556-4029</eissn><coden>JFSCAS</coden><abstract>Scanning electron microscopy combined with energy dispersive X-ray analysis (SEM/EDX) was used to identify the gunshot residue (GSR) particles discharged by lead-free Sintox ammunition. Sintox GSR particles are characterized by spheroidal particles mainly consisting of titanium (Ti) and zinc (Zn). The results obtained in this study are in agreement with the hypothesis that GSR particles are formed by rapid condensation and solidification of vaporized and molten primer and bullet materials as a result of sudden temperature quench. The surface morphology of Ti-Zn particles is an essential criterion for their identification as gunshot residue particles and for discrimination against Ti-Zn environmental particles.</abstract><cop>Mundelein, Ill</cop><pub>Callaghan and Co</pub><doi>10.1520/JFS13626J</doi><tpages>5</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0022-1198
ispartof Journal of forensic sciences, 1994-03, Vol.39 (2), p.532-536
issn 0022-1198
1556-4029
language eng
recordid cdi_astm_journals_10_1520_JFS13626J
source ASTM Journals
title The Identification of Gunshot Residue Particles from Lead-Free Sintox Ammunition
url http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T18%3A57%3A21IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_astm_&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=The%20Identification%20of%20Gunshot%20Residue%20Particles%20from%20Lead-Free%20Sintox%20Ammunition&rft.jtitle=Journal%20of%20forensic%20sciences&rft.au=Gunaratnam,%20L&rft.date=1994-03-01&rft.volume=39&rft.issue=2&rft.spage=532&rft.epage=536&rft.pages=532-536&rft.issn=0022-1198&rft.eissn=1556-4029&rft.coden=JFSCAS&rft_id=info:doi/10.1520/JFS13626J&rft_dat=%3Cproquest_astm_%3E1308646627%3C/proquest_astm_%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-a334t-4825dd368fd6929033689bebfacf8d3b79ecc021ee12af1b8d9771df5b3cc7f83%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_pqid=1308646627&rft_id=info:pmid/&rfr_iscdi=true