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Comparative research of plasma-assisted milling and traditional milling in synthesizing AIN

In this paper,traditional milling and discharge plasma-assisted milling are employed to synthesize aluminum nitride(AlN) powder at nanometer scale by milling the mixture of aluminum and lithium hydroxide monohydrate.AlN powders can be generated in traditional milling and plasma-assisted milling in a...

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Bibliographic Details
Published in:等离子体科学与技术:英文版 2017-06, Vol.19 (6), p.33-37
Main Author: 王森 王文春 刘志杰 杨德正
Format: Article
Language:English
Online Access:Get full text
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Summary:In this paper,traditional milling and discharge plasma-assisted milling are employed to synthesize aluminum nitride(AlN) powder at nanometer scale by milling the mixture of aluminum and lithium hydroxide monohydrate.AlN powders can be generated in traditional milling and plasma-assisted milling in an hour milling time.Differential thermal analysis curves show that the reaction temperature of the powders treated by plasma-assisted milling is lower than that of traditional milling.These results indicate that plasma-assisted milling has higher efficiency in the synthesis of AlN,getting smaller crystallite size and activating powder.Moreover,an optical emission spectrum is employed to demonstrate the active species in plasma.The different formation process of AlN in the two-milling process,and the promotion effects of plasma in the milling process are discussed.
ISSN:1009-0630
DOI:10.1088/2058-6272/aa62f8