Loading…
ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid
This work describes the highly efficient acetylation (acylation) of alcohols with acetic acid for the ester synthesis in the presence of newly designed a new composite zirconium (IV) chloride and magnesium catalyst which is used bimetallic acidic catalyst ZrCl 4 ‐Mg(ClO 4 ) 2 , which is formed by gr...
Saved in:
| Published in: | Bulletin of the Korean Chemical Society 2022-04, Vol.43 (4), p.570-576 |
|---|---|
| Main Authors: | , , , |
| Format: | Article |
| Language: | English |
| Citations: | Items that this one cites Items that cite this one |
| Online Access: | Get full text |
| Tags: |
Add Tag
No Tags, Be the first to tag this record!
|
| cited_by | cdi_FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123 |
|---|---|
| cites | cdi_FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123 |
| container_end_page | 576 |
| container_issue | 4 |
| container_start_page | 570 |
| container_title | Bulletin of the Korean Chemical Society |
| container_volume | 43 |
| creator | Alam, Mohammad Mujahid Atkore, Sandeep T. Kamble, Vinod T. Varala, Ravi |
| description | This work describes the highly efficient acetylation (acylation) of alcohols with acetic acid for the ester synthesis in the presence of newly designed a new composite zirconium (IV) chloride and magnesium catalyst which is used bimetallic acidic catalyst ZrCl
4
‐Mg(ClO
4
)
2
, which is formed by grinding ZrCl
4
and Mg(ClO
4
)
2
in the molar ratio of 1:2, respectively. Thus, the powder X‐ray diffraction, scanning electron microscopy, Brunauer–Emmett–Teller surface area, and thermogravimetric analysis of the ZrCl
4
, Mg(ClO
4
)
2
, and non‐calcined ZrCl
4
‐Mg(ClO
4
)
2
were recorded. In each case, structural analysis was carried by grinding the catalyst in mortar and pestle. |
| doi_str_mv | 10.1002/bkcs.12481 |
| format | article |
| fullrecord | <record><control><sourceid>crossref</sourceid><recordid>TN_cdi_crossref_primary_10_1002_bkcs_12481</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>10_1002_bkcs_12481</sourcerecordid><originalsourceid>FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123</originalsourceid><addsrcrecordid>eNpNkLFOwzAURS0EEqWw8AVvBKQU24njhA1FQJGKunRiiZyXuDF1a2RbQtn4BL6RLyEtDEzvPt2jOxxCLhmdMUr5bbPBMGM8K9gRmTDOy0SUWXn8L5-SsxDeRlZKLiZk8-orCxl8f369rOEKKrscv2vgcAdzs-7tAJ3WBk23i9CYbReVtQYB1RiGEEE7Dwq7OFgVjduB06Asut5Z-DCxP3Qjr9C05-REKxu6i787JavHh1U1TxbLp-fqfpGgzFmiqW5ULgquMWV5WXBEmbVNIWTZFFLxbKRayanItRaoaKYwbYVELEZcM55Oyc3vLHoXgu90_e7NVvmhZrTeW6r3luqDpfQHfRFaOw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid</title><source>Wiley</source><creator>Alam, Mohammad Mujahid ; Atkore, Sandeep T. ; Kamble, Vinod T. ; Varala, Ravi</creator><creatorcontrib>Alam, Mohammad Mujahid ; Atkore, Sandeep T. ; Kamble, Vinod T. ; Varala, Ravi</creatorcontrib><description>This work describes the highly efficient acetylation (acylation) of alcohols with acetic acid for the ester synthesis in the presence of newly designed a new composite zirconium (IV) chloride and magnesium catalyst which is used bimetallic acidic catalyst ZrCl
4
‐Mg(ClO
4
)
2
, which is formed by grinding ZrCl
4
and Mg(ClO
4
)
2
in the molar ratio of 1:2, respectively. Thus, the powder X‐ray diffraction, scanning electron microscopy, Brunauer–Emmett–Teller surface area, and thermogravimetric analysis of the ZrCl
4
, Mg(ClO
4
)
2
, and non‐calcined ZrCl
4
‐Mg(ClO
4
)
2
were recorded. In each case, structural analysis was carried by grinding the catalyst in mortar and pestle.</description><identifier>ISSN: 1229-5949</identifier><identifier>EISSN: 1229-5949</identifier><identifier>DOI: 10.1002/bkcs.12481</identifier><language>eng</language><ispartof>Bulletin of the Korean Chemical Society, 2022-04, Vol.43 (4), p.570-576</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123</citedby><cites>FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123</cites><orcidid>0000-0003-1585-3842 ; 0000-0002-6466-9454 ; 0000-0002-0668-9027</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Alam, Mohammad Mujahid</creatorcontrib><creatorcontrib>Atkore, Sandeep T.</creatorcontrib><creatorcontrib>Kamble, Vinod T.</creatorcontrib><creatorcontrib>Varala, Ravi</creatorcontrib><title>ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid</title><title>Bulletin of the Korean Chemical Society</title><description>This work describes the highly efficient acetylation (acylation) of alcohols with acetic acid for the ester synthesis in the presence of newly designed a new composite zirconium (IV) chloride and magnesium catalyst which is used bimetallic acidic catalyst ZrCl
4
‐Mg(ClO
4
)
2
, which is formed by grinding ZrCl
4
and Mg(ClO
4
)
2
in the molar ratio of 1:2, respectively. Thus, the powder X‐ray diffraction, scanning electron microscopy, Brunauer–Emmett–Teller surface area, and thermogravimetric analysis of the ZrCl
4
, Mg(ClO
4
)
2
, and non‐calcined ZrCl
4
‐Mg(ClO
4
)
2
were recorded. In each case, structural analysis was carried by grinding the catalyst in mortar and pestle.</description><issn>1229-5949</issn><issn>1229-5949</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNpNkLFOwzAURS0EEqWw8AVvBKQU24njhA1FQJGKunRiiZyXuDF1a2RbQtn4BL6RLyEtDEzvPt2jOxxCLhmdMUr5bbPBMGM8K9gRmTDOy0SUWXn8L5-SsxDeRlZKLiZk8-orCxl8f369rOEKKrscv2vgcAdzs-7tAJ3WBk23i9CYbReVtQYB1RiGEEE7Dwq7OFgVjduB06Asut5Z-DCxP3Qjr9C05-REKxu6i787JavHh1U1TxbLp-fqfpGgzFmiqW5ULgquMWV5WXBEmbVNIWTZFFLxbKRayanItRaoaKYwbYVELEZcM55Oyc3vLHoXgu90_e7NVvmhZrTeW6r3luqDpfQHfRFaOw</recordid><startdate>202204</startdate><enddate>202204</enddate><creator>Alam, Mohammad Mujahid</creator><creator>Atkore, Sandeep T.</creator><creator>Kamble, Vinod T.</creator><creator>Varala, Ravi</creator><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-1585-3842</orcidid><orcidid>https://orcid.org/0000-0002-6466-9454</orcidid><orcidid>https://orcid.org/0000-0002-0668-9027</orcidid></search><sort><creationdate>202204</creationdate><title>ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid</title><author>Alam, Mohammad Mujahid ; Atkore, Sandeep T. ; Kamble, Vinod T. ; Varala, Ravi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Alam, Mohammad Mujahid</creatorcontrib><creatorcontrib>Atkore, Sandeep T.</creatorcontrib><creatorcontrib>Kamble, Vinod T.</creatorcontrib><creatorcontrib>Varala, Ravi</creatorcontrib><collection>CrossRef</collection><jtitle>Bulletin of the Korean Chemical Society</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Alam, Mohammad Mujahid</au><au>Atkore, Sandeep T.</au><au>Kamble, Vinod T.</au><au>Varala, Ravi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid</atitle><jtitle>Bulletin of the Korean Chemical Society</jtitle><date>2022-04</date><risdate>2022</risdate><volume>43</volume><issue>4</issue><spage>570</spage><epage>576</epage><pages>570-576</pages><issn>1229-5949</issn><eissn>1229-5949</eissn><abstract>This work describes the highly efficient acetylation (acylation) of alcohols with acetic acid for the ester synthesis in the presence of newly designed a new composite zirconium (IV) chloride and magnesium catalyst which is used bimetallic acidic catalyst ZrCl
4
‐Mg(ClO
4
)
2
, which is formed by grinding ZrCl
4
and Mg(ClO
4
)
2
in the molar ratio of 1:2, respectively. Thus, the powder X‐ray diffraction, scanning electron microscopy, Brunauer–Emmett–Teller surface area, and thermogravimetric analysis of the ZrCl
4
, Mg(ClO
4
)
2
, and non‐calcined ZrCl
4
‐Mg(ClO
4
)
2
were recorded. In each case, structural analysis was carried by grinding the catalyst in mortar and pestle.</abstract><doi>10.1002/bkcs.12481</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0003-1585-3842</orcidid><orcidid>https://orcid.org/0000-0002-6466-9454</orcidid><orcidid>https://orcid.org/0000-0002-0668-9027</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1229-5949 |
| ispartof | Bulletin of the Korean Chemical Society, 2022-04, Vol.43 (4), p.570-576 |
| issn | 1229-5949 1229-5949 |
| language | eng |
| recordid | cdi_crossref_primary_10_1002_bkcs_12481 |
| source | Wiley |
| title | ZrCl 4 ‐Mg ( ClO 4 ) 2 : Highly efficient bimetallic catalyst for acetylation of alcohol with acetic acid |
| url | http://sfxeu10.hosted.exlibrisgroup.com/loughborough?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-29T19%3A50%3A17IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-crossref&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=ZrCl%204%20%E2%80%90Mg%20(%20ClO%204%20)%202%20:%20Highly%20efficient%20bimetallic%20catalyst%20for%20acetylation%20of%20alcohol%20with%20acetic%20acid&rft.jtitle=Bulletin%20of%20the%20Korean%20Chemical%20Society&rft.au=Alam,%20Mohammad%20Mujahid&rft.date=2022-04&rft.volume=43&rft.issue=4&rft.spage=570&rft.epage=576&rft.pages=570-576&rft.issn=1229-5949&rft.eissn=1229-5949&rft_id=info:doi/10.1002/bkcs.12481&rft_dat=%3Ccrossref%3E10_1002_bkcs_12481%3C/crossref%3E%3Cgrp_id%3Ecdi_FETCH-LOGICAL-c761-f0fba6582fc316982cc74db8579b87a24c76d72056ff5ca04ac3d57cc8316f123%3C/grp_id%3E%3Coa%3E%3C/oa%3E%3Curl%3E%3C/url%3E&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |