Synthesis of new 1,3-thiazepine derivatives

Condensation of thiourea derivatives with 1,4‐dibromobutane gave 1,3‐thiazepine derivatives (1a, 1b, 1c − 3a, 3b, 3c). Elementary analysis, MS and 1H NMR spectra confirmed the identity of the products. The molecular structure of 2b was determined by an X‐ray analysis. J. Heterocyclic Chem., (2009)....

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Published in:Journal of heterocyclic chemistry 2009-03, Vol.46 (2), p.298-302
Main Authors: Struga, Marta, Kossakowski, Jerzy, Miroslaw, Barbara, Koziol, Anna E., Zimniak, Andrzej
Format: Article
Language:English
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Summary:Condensation of thiourea derivatives with 1,4‐dibromobutane gave 1,3‐thiazepine derivatives (1a, 1b, 1c − 3a, 3b, 3c). Elementary analysis, MS and 1H NMR spectra confirmed the identity of the products. The molecular structure of 2b was determined by an X‐ray analysis. J. Heterocyclic Chem., (2009).
ISSN:0022-152X
1943-5193
DOI:10.1002/jhet.44