A practical laboratory route to the synthesis of trideuteriomethyl-[13C] iodide

A practical synthetic laboratory route for the synthesis of trideuteriomethyl‐[13C] iodide (13CD3I) (from tetradeuterio‐[13C]‐methanol and hydriodic acid) is described. We comment on the experimental protocol, and the use of water as an ‘additive’ to improve the synthetic yield. Copyright © 2003 Joh...

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Bibliographic Details
Published in:Journal of labelled compounds & radiopharmaceuticals 2003-03, Vol.46 (4), p.291-296
Main Authors: Coumbarides, Gregory S., Eames, Jason, Weerasooriya, Neluka
Format: Article
Language:English
Subjects:
Aliphatic compounds
Carbon-13 and Trideuterio-[13C]-methyl iodide
Chemistry
Deuterium
Exact sciences and technology
Organic chemistry
Preparations and properties
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Summary:A practical synthetic laboratory route for the synthesis of trideuteriomethyl‐[13C] iodide (13CD3I) (from tetradeuterio‐[13C]‐methanol and hydriodic acid) is described. We comment on the experimental protocol, and the use of water as an ‘additive’ to improve the synthetic yield. Copyright © 2003 John Wiley & Sons, Ltd.
ISSN:0362-4803
1099-1344
DOI:10.1002/jlcr.666