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Complexes of N ‐Thiophosphorylthiourea t BuNHC(S)NHP(S)(O i Pr) 2 with Zinc(II), Cadmium(II), Nickel(II), and Cobalt(II) Cations
Reaction of the potassium salt of N ‐thiophosphorylthiourea t BuNHC(S)NHP(S)(O i Pr) 2 ( HL ) with Zn II , Cd II , Ni II and Co II in aqueous EtOH leads to complexes of common formula M(L‐ S,S′ ) 2 ( ML 2 ). Complexes were investigated by IR, UV‐Vis, 1 H and 31 P{ 1 H} NMR spectroscopy and microanal...
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| Published in: | Zeitschrift für anorganische und allgemeine Chemie (1950) 2008-05, Vol.634 (5), p.967-971 |
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| Main Authors: | , , , , , , , |
| Format: | Article |
| Language: | English |
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| cites | cdi_FETCH-LOGICAL-c849-d8b5549ea0e787e49adb0797ead8e4532a7a5bf17ea89684bcc3b319b46c49dd3 |
| container_end_page | 971 |
| container_issue | 5 |
| container_start_page | 967 |
| container_title | Zeitschrift für anorganische und allgemeine Chemie (1950) |
| container_volume | 634 |
| creator | Safin, Damir A. Sokolov, Felix D. Gimadiev, Timur R. Brusko, Vasiliy V. Babashkina, Maria G. Chubukaeva, Dinara R. Krivolapov, Dmitriy B. Litvinov, Igor A. |
| description | Reaction of the potassium salt of
N
‐thiophosphorylthiourea
t
BuNHC(S)NHP(S)(O
i
Pr)
2
(
HL
) with Zn
II
, Cd
II
, Ni
II
and Co
II
in aqueous EtOH leads to complexes of common formula M(L‐
S,S′
)
2
(
ML
2
). Complexes were investigated by IR, UV‐Vis,
1
H and
31
P{
1
H} NMR spectroscopy and microanalysis The structure of complex
NiL
2
was investigated by single crystal X‐ray diffraction analysis. The nickel(II) ion has a squre‐planar environment, S
4
, with two anionic ligands involving 1,5‐S,S′‐coordination mode. The ligands are bound in a
trans
configuration. |
| doi_str_mv | 10.1002/zaac.200700549 |
| format | article |
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N
‐thiophosphorylthiourea
t
BuNHC(S)NHP(S)(O
i
Pr)
2
(
HL
) with Zn
II
, Cd
II
, Ni
II
and Co
II
in aqueous EtOH leads to complexes of common formula M(L‐
S,S′
)
2
(
ML
2
). Complexes were investigated by IR, UV‐Vis,
1
H and
31
P{
1
H} NMR spectroscopy and microanalysis The structure of complex
NiL
2
was investigated by single crystal X‐ray diffraction analysis. The nickel(II) ion has a squre‐planar environment, S
4
, with two anionic ligands involving 1,5‐S,S′‐coordination mode. The ligands are bound in a
trans
configuration.</description><identifier>ISSN: 0044-2313</identifier><identifier>EISSN: 1521-3749</identifier><identifier>DOI: 10.1002/zaac.200700549</identifier><language>eng</language><ispartof>Zeitschrift für anorganische und allgemeine Chemie (1950), 2008-05, Vol.634 (5), p.967-971</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c849-d8b5549ea0e787e49adb0797ead8e4532a7a5bf17ea89684bcc3b319b46c49dd3</citedby><cites>FETCH-LOGICAL-c849-d8b5549ea0e787e49adb0797ead8e4532a7a5bf17ea89684bcc3b319b46c49dd3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Safin, Damir A.</creatorcontrib><creatorcontrib>Sokolov, Felix D.</creatorcontrib><creatorcontrib>Gimadiev, Timur R.</creatorcontrib><creatorcontrib>Brusko, Vasiliy V.</creatorcontrib><creatorcontrib>Babashkina, Maria G.</creatorcontrib><creatorcontrib>Chubukaeva, Dinara R.</creatorcontrib><creatorcontrib>Krivolapov, Dmitriy B.</creatorcontrib><creatorcontrib>Litvinov, Igor A.</creatorcontrib><title>Complexes of N ‐Thiophosphorylthiourea t BuNHC(S)NHP(S)(O i Pr) 2 with Zinc(II), Cadmium(II), Nickel(II), and Cobalt(II) Cations</title><title>Zeitschrift für anorganische und allgemeine Chemie (1950)</title><description>Reaction of the potassium salt of
N
‐thiophosphorylthiourea
t
BuNHC(S)NHP(S)(O
i
Pr)
2
(
HL
) with Zn
II
, Cd
II
, Ni
II
and Co
II
in aqueous EtOH leads to complexes of common formula M(L‐
S,S′
)
2
(
ML
2
). Complexes were investigated by IR, UV‐Vis,
1
H and
31
P{
1
H} NMR spectroscopy and microanalysis The structure of complex
NiL
2
was investigated by single crystal X‐ray diffraction analysis. The nickel(II) ion has a squre‐planar environment, S
4
, with two anionic ligands involving 1,5‐S,S′‐coordination mode. The ligands are bound in a
trans
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N
‐thiophosphorylthiourea
t
BuNHC(S)NHP(S)(O
i
Pr)
2
(
HL
) with Zn
II
, Cd
II
, Ni
II
and Co
II
in aqueous EtOH leads to complexes of common formula M(L‐
S,S′
)
2
(
ML
2
). Complexes were investigated by IR, UV‐Vis,
1
H and
31
P{
1
H} NMR spectroscopy and microanalysis The structure of complex
NiL
2
was investigated by single crystal X‐ray diffraction analysis. The nickel(II) ion has a squre‐planar environment, S
4
, with two anionic ligands involving 1,5‐S,S′‐coordination mode. The ligands are bound in a
trans
configuration.</abstract><doi>10.1002/zaac.200700549</doi><tpages>5</tpages></addata></record> |
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| issn | 0044-2313 1521-3749 |
| language | eng |
| recordid | cdi_crossref_primary_10_1002_zaac_200700549 |
| source | Wiley-Blackwell Read & Publish Collection |
| title | Complexes of N ‐Thiophosphorylthiourea t BuNHC(S)NHP(S)(O i Pr) 2 with Zinc(II), Cadmium(II), Nickel(II), and Cobalt(II) Cations |
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