Automatic Injection Analysis with Chemiluminescence Detection: Determination of Hydrazine

Luminous oxidation with acidic permanganate was found to be usable for chemiluminescence determination of hydrazine and its derivatives. The sensitivity is high enough to determine hydrazine in workroom air. The effects of various compounds, especially metal ions, and of temperature and mixing order...

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Bibliographic Details
Published in:Microchemical journal 1996-04, Vol.53 (3), p.356-360
Main Authors: He, Zhike, Liu, Xinglian, Luo, Qingyao, Tang, Hongwu, Yu, Ximao, Chen, Hui, Zeng, Yun'e
Format: Article
Language:English
Subjects:
Analytical chemistry
Chemical and thermal methods
Chemistry
Exact sciences and technology
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Summary:Luminous oxidation with acidic permanganate was found to be usable for chemiluminescence determination of hydrazine and its derivatives. The sensitivity is high enough to determine hydrazine in workroom air. The effects of various compounds, especially metal ions, and of temperature and mixing order on the procedure were investigated. The linear range is 3.0 × 10−5− 1.0 × 10−7g/ml. The chemiluminescence mechanism is discussed.
ISSN:0026-265X
1095-9149
DOI:10.1006/mchj.1996.0051