Development of an HPLC-NMR method for the determination of PAHs in soil samples - a comparison with conventional methods

A hyphenated HPLC-(1)H NMR method for the identification and quantification of PAHs in soil samples has been developed and applied to a PAH reference sample provided by the Federal Institute for Materials Research and Testing (BAM, Berlin, Germany). The results were compared with those obtained by H...

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Bibliographic Details
Published in:Analytical and bioanalytical chemistry 2002-08, Vol.373 (8), p.810-819
Main Authors: Weisshoff, Hardy, Preiss, Alfred, Nehls, Irene, Win, Tin, Mügge, Clemens
Format: Article
Language:English
Subjects:
Chromatography, High Pressure Liquid - methods
Gas Chromatography-Mass Spectrometry
Magnetic Resonance Spectroscopy - methods
Polycyclic Compounds - analysis
Reference Standards
Sensitivity and Specificity
Soil Pollutants - analysis
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Summary:A hyphenated HPLC-(1)H NMR method for the identification and quantification of PAHs in soil samples has been developed and applied to a PAH reference sample provided by the Federal Institute for Materials Research and Testing (BAM, Berlin, Germany). The results were compared with those obtained by HPLC-DAD, HPLC-F, and GC-MS analyses of the same sample.
ISSN:1618-2642
1618-2650
DOI:10.1007/s00216-002-1407-7