Synthesis of N,N-dialkylnitramines from secondary ammonium nitrates in liquid or supercritical carbon dioxide

An efficient explosion-proof method was developed for the preparation of N,N -dialkylnitramines by treatment of dialkylammonium nitrates with a mixture of nitric acid and acetic anhydride in the presence of ZnCl 2 in liduid or supercritical carbon dioxide.

Saved in:
Bibliographic Details
Published in:Russian chemical bulletin 2009-10, Vol.58 (10), p.2058-2062
Main Authors: Kuchurov, I. V., Fomenkov, I. V., Zlotin, S. G.
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Full Articles
Inorganic Chemistry
Organic Chemistry
Citations: Items that this one cites
Items that cite this one
Online Access:Get full text
Tags: Add Tag
No Tags, Be the first to tag this record!
Description
Summary:An efficient explosion-proof method was developed for the preparation of N,N -dialkylnitramines by treatment of dialkylammonium nitrates with a mixture of nitric acid and acetic anhydride in the presence of ZnCl 2 in liduid or supercritical carbon dioxide.
ISSN:1066-5285
1573-9171
DOI:10.1007/s11172-009-0282-1