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First optically active P-alkoxy derivative of palladated phosphacymantrene: synthesis, structure, and chiroptical properties
The solvopalladation reaction of 2,5-diphenylphosphacymantrene with Na 2 PdCl 4 , AcONa, and optically active carbinol ( S )-(−)-2-methylbutanol was carried out. Optically active complex 3 was obtained and characterized by X-ray diffraction analysis and circular dichroism (CD), 13 C and 31 P NMR, IR...
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| Published in: | Russian chemical bulletin 2013-04, Vol.62 (4), p.1080-1085 |
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| Main Authors: | , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c288t-d0775981446ac2c226cd36a60a15d08dee6788badf6c0f01170cf1c2cd42f2d03 |
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| cites | cdi_FETCH-LOGICAL-c288t-d0775981446ac2c226cd36a60a15d08dee6788badf6c0f01170cf1c2cd42f2d03 |
| container_end_page | 1085 |
| container_issue | 4 |
| container_start_page | 1080 |
| container_title | Russian chemical bulletin |
| container_volume | 62 |
| creator | Smol’yakov, A. F. Ginzburg, A. G. Bashilov, V. V. Dolgushin, F. M. Petrovskii, P. V. Babievsky, K. K. Sokolov, V. I. |
| description | The solvopalladation reaction of 2,5-diphenylphosphacymantrene with Na
2
PdCl
4
, AcONa, and optically active carbinol (
S
)-(−)-2-methylbutanol was carried out. Optically active complex
3
was obtained and characterized by X-ray diffraction analysis and circular dichroism (CD),
13
C and
31
P NMR, IR, and UV spectra. |
| doi_str_mv | 10.1007/s11172-013-0145-7 |
| format | article |
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2
PdCl
4
, AcONa, and optically active carbinol (
S
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13
C and
31
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2
PdCl
4
, AcONa, and optically active carbinol (
S
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13
C and
31
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2
PdCl
4
, AcONa, and optically active carbinol (
S
)-(−)-2-methylbutanol was carried out. Optically active complex
3
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13
C and
31
P NMR, IR, and UV spectra.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s11172-013-0145-7</doi><tpages>6</tpages></addata></record> |
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| ispartof | Russian chemical bulletin, 2013-04, Vol.62 (4), p.1080-1085 |
| issn | 1066-5285 1573-9171 |
| language | eng |
| recordid | cdi_crossref_primary_10_1007_s11172_013_0145_7 |
| source | Springer Nature |
| subjects | Chemistry Chemistry and Materials Science Chemistry/Food Science Full Articles Inorganic Chemistry Organic Chemistry |
| title | First optically active P-alkoxy derivative of palladated phosphacymantrene: synthesis, structure, and chiroptical properties |
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