Synthesis and characterization of CdS and CdSe nanoparticles prepared from novel intramolecularly stabilized single-source precursors

In this note we describe the synthesis of cadmium sulphide and selenide nanoparticles from the corresponding novel single source precursors, M[E(Ox)] 2 [E = S (1), Se (2); M = Cd; Ox = 2-(4,4-dimethyl-2-oxazolinyl)benzene] by thermolysing in tri- n -octylphosphine oxide (TOPO) at 280 °C, and their c...

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Bibliographic Details
Published in:Journal of chemical sciences (Bangalore, India) India), 2009-05, Vol.121 (3), p.293-296
Main Authors: Kandasamy, Karuppasamy, Singh, Harkesh B., Kulshreshtha, Shailendra K.
Format: Article
Language:English
Subjects:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
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Summary:In this note we describe the synthesis of cadmium sulphide and selenide nanoparticles from the corresponding novel single source precursors, M[E(Ox)] 2 [E = S (1), Se (2); M = Cd; Ox = 2-(4,4-dimethyl-2-oxazolinyl)benzene] by thermolysing in tri- n -octylphosphine oxide (TOPO) at 280 °C, and their characterization by X-ray powder diffraction (XRD), transmission electron microscope (TEM) and scanning electron microscope (SEM) studies.
ISSN:0974-3626
0973-7103
DOI:10.1007/s12039-009-0032-9