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Chemical synthesis, structural characterization and optical properties of nanophase α-Ag2WO4

Silver tungstate ( α -Ag 2 WO 4 ) nanoparticles were synthesized by chemical precipitation method. Thermodynamic stability of the α -Ag 2 WO 4 nanoparticles was studied by thermogravimetric and differential thermal analysis. These nanoparticles were structurally characterized by X-ray diffraction, F...

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Bibliographic Details
Published in:Indian journal of physics 2015-09, Vol.89 (9), p.889-897
Main Authors: Sreedevi, A., Priyanka, K. P., Babitha, K. K., Aloysius Sabu, N., Anu, T. S., Varghese, T.
Format: Article
Language:English
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Summary:Silver tungstate ( α -Ag 2 WO 4 ) nanoparticles were synthesized by chemical precipitation method. Thermodynamic stability of the α -Ag 2 WO 4 nanoparticles was studied by thermogravimetric and differential thermal analysis. These nanoparticles were structurally characterized by X-ray diffraction, Fourier transform infrared spectroscopy and Raman spectroscopy. The structure and morphology of these nanoparticles were studied by scanning electron microscopy and high-resolution transmission electron microscopy. The composition of nanoparticles near and at the surface was estimated by using energy-dispersive X-ray analysis. The optical properties of these nanoparticles were investigated by UV–Visible as well as photoluminescence spectroscopy. The effects of calcination temperature on the geometric parameters and optical properties of α -Ag 2 WO 4 nanoparticle samples was also investigated.
ISSN:0973-1458
0974-9845
DOI:10.1007/s12648-015-0664-1