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Chemical synthesis, structural characterization and optical properties of nanophase α-Ag2WO4
Silver tungstate ( α -Ag 2 WO 4 ) nanoparticles were synthesized by chemical precipitation method. Thermodynamic stability of the α -Ag 2 WO 4 nanoparticles was studied by thermogravimetric and differential thermal analysis. These nanoparticles were structurally characterized by X-ray diffraction, F...
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Published in: | Indian journal of physics 2015-09, Vol.89 (9), p.889-897 |
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Main Authors: | , , , , , |
Format: | Article |
Language: | English |
Subjects: | |
Citations: | Items that this one cites Items that cite this one |
Online Access: | Get full text |
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Summary: | Silver tungstate (
α
-Ag
2
WO
4
) nanoparticles were synthesized by chemical precipitation method. Thermodynamic stability of the
α
-Ag
2
WO
4
nanoparticles was studied by thermogravimetric and differential thermal analysis. These nanoparticles were structurally characterized by X-ray diffraction, Fourier transform infrared spectroscopy and Raman spectroscopy. The structure and morphology of these nanoparticles were studied by scanning electron microscopy and high-resolution transmission electron microscopy. The composition of nanoparticles near and at the surface was estimated by using energy-dispersive X-ray analysis. The optical properties of these nanoparticles were investigated by UV–Visible as well as photoluminescence spectroscopy. The effects of calcination temperature on the geometric parameters and optical properties of
α
-Ag
2
WO
4
nanoparticle samples was also investigated. |
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ISSN: | 0973-1458 0974-9845 |
DOI: | 10.1007/s12648-015-0664-1 |