Improvements of analytical results of thermal ionization mass spectrometry through electrolytic sample deposition

A method of sample deposition based on electrodeposition in a dimethyl formamide media is proposed. The apparatus and procedure described lead to centered and reproducible deposits on three filaments assemblies. The same procedure is used for all the actinides. The electrodeposition yields range fro...

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Bibliographic Details
Published in:International journal of mass spectrometry and ion physics 1983, Vol.48, p.393-396
Main Authors: Bergey, C., Cesario, J., Deniaud, S.
Format: Article
Language:English
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Summary:A method of sample deposition based on electrodeposition in a dimethyl formamide media is proposed. The apparatus and procedure described lead to centered and reproducible deposits on three filaments assemblies. The same procedure is used for all the actinides. The electrodeposition yields range from 40 to 90 %. Mass spectrometry results demonstrate improved precision and better sensitivity. The simplicity of manipulations allows easy automation.
ISSN:0020-7381
1873-3034
DOI:10.1016/0020-7381(83)87110-1