High-performance liquid chromatographic separation of chiral metallocenic ketones and alcohols

The enantiomers of chiral (arene)tricarbonylchromium ketones and alcohols were separated by high-performance liquid chromatography with a Chiralcel OD column. The absolute configuration of the ketones was assigned on the basis of the sign of optical rotation determined with an on-line detector.

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Bibliographic Details
Published in:Journal of Chromatography A 1992-05, Vol.600 (2), p.320-322
Main Authors: Carrea, G., Pasta, P., Colonna, S., Gaggero, N.
Format: Article
Language:English
Subjects:
Analytical chemistry
Chemistry
Chromatographic methods and physical methods associated with chromatography
Exact sciences and technology
Other chromatographic methods
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Description
Summary:The enantiomers of chiral (arene)tricarbonylchromium ketones and alcohols were separated by high-performance liquid chromatography with a Chiralcel OD column. The absolute configuration of the ketones was assigned on the basis of the sign of optical rotation determined with an on-line detector.
ISSN:0021-9673
DOI:10.1016/0021-9673(92)85565-B