Correlation of 13C and 1H chemical shifts in bovine high-density lipoprotein from two-dimensional NMR

Two-dimensional heteronuclear 13C 1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at t...

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Bibliographic Details
Published in:Journal of magnetic resonance (1969) 1984-09, Vol.59 (2), p.268-274
Main Authors: Coffin, Scott, Limm, Mona, Cowburn, David
Format: Article
Language:English
Subjects:
Biological and medical sciences
Fundamental and applied biological sciences. Psychology
Molecular biophysics
Spectroscopy : techniques and spectras
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Summary:Two-dimensional heteronuclear 13C 1H chemical-shift correlation spectra were obtained for bovine high-density lipoprotein (HDL). The 13C and 1H shifts of the lipid components are assigned. No evidence for dynamic equilibration of lipid classes between different structure environments was found at this limited resolution. Heteronuclear correlation spectroscopy can be effectively applied to macromolecular complexes as large as HDLs.
ISSN:0022-2364
1557-8968
DOI:10.1016/0022-2364(84)90171-9