Limitations of a self-integrating method for the simultaneous C, H, and N determination by thermal conductivity measurement

Limitations and ultimate performance of a fully automatic carbon, hydrogen, and nitrogen analyzer with a self-integrating thermal conductivity finish are discussed. It is shown that a simultaneous carbon, hydrogen, and nitrogen determination on a sample of 1 mg burned in a static system of oxygen is...

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Bibliographic Details
Published in:Microchemical journal 1963-01, Vol.7 (4), p.422-436
Main Authors: Clerc, J.T., Simon, W.
Format: Article
Language:English
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Summary:Limitations and ultimate performance of a fully automatic carbon, hydrogen, and nitrogen analyzer with a self-integrating thermal conductivity finish are discussed. It is shown that a simultaneous carbon, hydrogen, and nitrogen determination on a sample of 1 mg burned in a static system of oxygen is possible with a standard error of 0.13, 0.07, and 0.18%, respectively. One determination takes 13 minutes.
ISSN:0026-265X
1095-9149
DOI:10.1016/0026-265X(63)90076-6