A new generation of track etched membranes for microfiltration and ultrafiltration. Part I. Preparation and characterisation

A new experimental apparatus for porous track etched membrane production has been designed, tested and installed near the core of the IEA-R1 nuclear reactor at IPEN-Sao Paulo. The thermal neutron flux close to the centre of the reactor core has been used to produce fission fragments from uranium sam...

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Bibliographic Details
Published in:Journal of membrane science 1996-09, Vol.118 (2), p.239-245
Main Authors: Yamazaki, Ione M., Paterson, Russell, Geraldo, Luiz Paulo
Format: Article
Language:English
Subjects:
Chemistry
Colloidal state and disperse state
Exact sciences and technology
Fission fragments
General and physical chemistry
Membranes
Microfiltration
Polycarbonate
Porous membrane
Track etch
Ultrafiltration
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Summary:A new experimental apparatus for porous track etched membrane production has been designed, tested and installed near the core of the IEA-R1 nuclear reactor at IPEN-Sao Paulo. The thermal neutron flux close to the centre of the reactor core has been used to produce fission fragments from uranium sample which was deposited on a rod located at the centre of an evacuated aluminium chamber. These nuclear fragments impinge on a polycarbonate film mounted on the inner cylindrical wall of the irradiation chamber. Under conditions of uniform neutron flux large areas of track etched membranes, with high level of pore uniformity, have been produced in the micro and ultrafiltration range. Membranes with pore diameters ranging from 15 to 100 nm. have been prepared reproducibly, based upon a calibration curve of track diameter versus etching time.
ISSN:0376-7388
1873-3123
DOI:10.1016/0376-7388(96)00098-1