Fluorescence characterization and identification of polynuclear aromatic hydrocarbons in shale oil

Fluorescence spectrometry, dry-column chromatography, and thin-layer chromatography are combined to separate, characterize and identify rapidly polynuclear aromatic hydrocarbons in shale oil. The fluorescence profile of separated fluorescent components is obtained directly on a chromatoplate and a s...

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Bibliographic Details
Published in:Analytica chimica acta 1977-01, Vol.89 (2), p.377-382
Main Authors: Hurtubise, R.J., Schabron, J.F., Feaster, J.D., Therkildsen, D.H., Poulson, R.E.
Format: Article
Language:English
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Summary:Fluorescence spectrometry, dry-column chromatography, and thin-layer chromatography are combined to separate, characterize and identify rapidly polynuclear aromatic hydrocarbons in shale oil. The fluorescence profile of separated fluorescent components is obtained directly on a chromatoplate and a semi-quantitative determination of polynuclear aromatic hydrocarbons in shale oil is discussed. Pyrene and benzo-[α]-pyrene can be identified by order of elution on a dry column, R F value on a chromatoplate, color of fluorescence, and fluorescence excitation and emission spectra.
ISSN:0003-2670
1873-4324
DOI:10.1016/S0003-2670(01)84735-8