Growth, spectroscopic and thermal behavior of Cd(SCN) 2(DMSO) 2

Single crystals of the organometallic material, bis(dimethyl sulfoxide) cadmium thiocyanate (DSTC), Cd(SCN) 2(DMSO) 2 were grown from aqueous solution. The grown crystals were characterized by elemental analyses, X-ray powder diffraction, Raman, infrared and optical transmission spectroscopy and the...

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Bibliographic Details
Published in:Journal of crystal growth 2002-12, Vol.246 (1), p.155-160
Main Authors: Wang, X.Q, Xu, D, Yuan, D.R, Lu, M.K, Cheng, X.F, Huang, J, Lu, G.W, Guo, S.Y, Zhang, G.H
Format: Article
Language:English
Subjects:
A1. Characterization
A1. Solvents
A1. X-ray powder diffraction
A2. Growth from solutions
A2. Single crystal growth
B1. Cadmium compounds
Cross-disciplinary physics: materials science
rheology
Exact sciences and technology
Growth from solutions
Materials science
Methods of crystal growth
physics of crystal growth
Physics
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Summary:Single crystals of the organometallic material, bis(dimethyl sulfoxide) cadmium thiocyanate (DSTC), Cd(SCN) 2(DMSO) 2 were grown from aqueous solution. The grown crystals were characterized by elemental analyses, X-ray powder diffraction, Raman, infrared and optical transmission spectroscopy and thermal analysis. The UV transparency cutoff of DSTC crystal is 263 nm. It exhibits good physicochemical stability up to 134°C, and the final residue of thermal decomposition is CdS.
ISSN:0022-0248
1873-5002
DOI:10.1016/S0022-0248(02)01763-3