4-(2,2-dimethyldioxalan-4-yl)-5-(quinoxalin-2-yl)-1,3-dithiol-2-one, a proligand relating to the cofactor of the oxomolybdoenzymes

The coupling of 2-iodoquinoxaline to 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(tri- n-butylstannyl)-1,3-dithiol-2-one 5 gave 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(quinoxalin-2-yl)-1,3-dithiol-2-one 4. The coupling of 2-iodoquinoxaline to 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(tri-n-butylstannyl)-1,3-dith...

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Bibliographic Details
Published in:Tetrahedron 1998-03, Vol.54 (13), p.3291-3302
Main Authors: Dinsmore, Andrew, David Garner, C., Joule, John A.
Format: Article
Language:English
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Summary:The coupling of 2-iodoquinoxaline to 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(tri- n-butylstannyl)-1,3-dithiol-2-one 5 gave 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(quinoxalin-2-yl)-1,3-dithiol-2-one 4. The coupling of 2-iodoquinoxaline to 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(tri-n-butylstannyl)-1,3-dithiole-2-one gave 4-(2,2-dimethyl-1,3-dioxolan-4-yl)-5-(quinoxalin-2-yl)-1,3-dithiol-2-one.
ISSN:0040-4020
1464-5416
DOI:10.1016/S0040-4020(98)00072-6