The novel product of cathodic reduction of phthalimide anion

Cathodic reduction of phthalimide anion in methanol was studied. The novel product, N-hydroxymethyl-3-hydroxyphthalimidine, was found. Full characterization of this new compound was carried out by means of NMR, FT-IR, MS, and X-ray crystallography. The mechanism of electrolytic formation of N-hydrox...

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Bibliographic Details
Published in:Tetrahedron 1998-06, Vol.54 (26), p.7517-7524
Main Authors: Orzeszko, Andrzej, Maurin, Jan K., Niedźwiecka-Kornaś, Anna, Kazimierczuk, Zygmunt
Format: Article
Language:English
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Summary:Cathodic reduction of phthalimide anion in methanol was studied. The novel product, N-hydroxymethyl-3-hydroxyphthalimidine, was found. Full characterization of this new compound was carried out by means of NMR, FT-IR, MS, and X-ray crystallography. The mechanism of electrolytic formation of N-hydroxymethyl-3-hydroxyphthalimidine is proposed. Cathodic reduction of phthalimide anion in methanol was studied. The novel product, N-hydroxy-methyl-3-hydroxyphthalimidine, was found.
ISSN:0040-4020
1464-5416
DOI:10.1016/S0040-4020(98)00386-X