Cyclopropanation by tandem radical [2 + 1] cycloaddition conducted by nickel complexes catalyzed electroreduction

Bicyclo[3. 1. 0]-, 3-azabicyclo [3. 1. 0]- and 3-oxabicyclo[3. 1. 0]hexane derivatives were prepared by a nickel complex catalyzed elctroreduction of 2-bromo or 2-iodo-1, 6-diene derivatives. Nickel complexes catalyzed electroreduction of 2-halo-1,6-dienes lead to bicyclo[3. 1. 0]skeletons.

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Bibliographic Details
Published in:Tetrahedron letters 1997-04, Vol.38 (15), p.2705-2708
Main Authors: Ozaki, Shigeko, Matsui, Eiki, Waku, Junya, Ohmori, Hidenobu
Format: Article
Language:English
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Summary:Bicyclo[3. 1. 0]-, 3-azabicyclo [3. 1. 0]- and 3-oxabicyclo[3. 1. 0]hexane derivatives were prepared by a nickel complex catalyzed elctroreduction of 2-bromo or 2-iodo-1, 6-diene derivatives. Nickel complexes catalyzed electroreduction of 2-halo-1,6-dienes lead to bicyclo[3. 1. 0]skeletons.
ISSN:0040-4039
1873-3581
DOI:10.1016/S0040-4039(97)00434-6