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Experimental study of the production of high purity ethanol using a semi-continuous extractive batch dividing wall distillation column

Experimental DWDC used for the production of high purity bioethanol. [Display omitted] •Purification of ethanol using an experimental dividing wall distillation column.•Use of glycerol as entrainer for obtaining high purity ethanol.•Semicontinuous operation of a dividing wall column. In this paper,...

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Published in:Chemical engineering and processing 2016-10, Vol.108, p.74-77
Main Authors: García-Ventura, Ulises Miguel, Barroso-Muñoz, Fabricio Omar, Hernández, Salvador, Castro-Montoya, Agustín Jaime
Format: Article
Language:English
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Summary:Experimental DWDC used for the production of high purity bioethanol. [Display omitted] •Purification of ethanol using an experimental dividing wall distillation column.•Use of glycerol as entrainer for obtaining high purity ethanol.•Semicontinuous operation of a dividing wall column. In this paper, the production of high purity ethanol using an experimental dividing wall distillation column using glycerol as entrainer is studied considering batch and semi-continuous operations. In the semi-continuous distillation, an ethanol-water mixture of composition 92% wt. ethanol was introduced in the pot and the glycerol was supplied through a continuous feed near to the top of the distillation column, it was possible to produce a distillate with a composition higher than 99% wt. ethanol. This result is important since it is possible to use this ethanol mixed with gasoline in the current motor vehicles operated with gasoline.
ISSN:0255-2701
1873-3204
DOI:10.1016/j.cep.2016.07.014