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Robust effectiveness behavior of synthesized cobalt doped Prussian blue graphene oxide ferrite against EMI shielding

[Display omitted] •Wide range of Electromagnetic Interference Shielding range.•High Value of Shielding at wide range of Frequency.•High Value of Shielding Absorption.•High Value of Shielding Reflection.•Usable for Shielding Applications. The new age demands high thermal stability, lightweight, and s...

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Published in:Inorganic chemistry communications 2022-03, Vol.137, p.109204, Article 109204
Main Authors: Ali, Muhammad Danish, Aslam, Ammara, Zeeshan, Talat, Mubaraka, Rafia, Bukhari, Syed Aashir, Shoaib, Muhammad, Amami, Mongi, Farhat, Iamia ben, Ahmed, Samia ben, Abdelhak, Jawher, Waseem, Salma
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cited_by cdi_FETCH-LOGICAL-c306t-6e563e00626833136aae13fb67a26b24d6802aaebe56b87559b31fb78f21c5353
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container_start_page 109204
container_title Inorganic chemistry communications
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creator Ali, Muhammad Danish
Aslam, Ammara
Zeeshan, Talat
Mubaraka, Rafia
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Shoaib, Muhammad
Amami, Mongi
Farhat, Iamia ben
Ahmed, Samia ben
Abdelhak, Jawher
Waseem, Salma
description [Display omitted] •Wide range of Electromagnetic Interference Shielding range.•High Value of Shielding at wide range of Frequency.•High Value of Shielding Absorption.•High Value of Shielding Reflection.•Usable for Shielding Applications. The new age demands high thermal stability, lightweight, and strong absorptivity EM shielding materials with a broad absorption range of frequency band. The graphene oxide (GO) was synthesized through Hummer's method. Cobalt ferrite (COF) synthesized through the hydrothermal process and Prussian blue graphene oxide cobalt ferrite (PBGOCOF) synthesized through in-situ technique. The material formation confirmed through XRD and peaks are detected at 24.75°, 29.95°, 35.32°, 39.94°, 42.95°, 50.11°, 54.6°, 57.08° and 59.2° with corresponding crystal planes (111) (220) (311) (420) (422) (440) (600) (620) and (511) reflections. The epoxy, alkoxy, carboxyl, and O-H bonding was calculated through FTIR spectroscopy, and by using different bonding the material was characterized. Raman spectroscopy was used to analyze the chemical structure of the graphene and PBGOCOF. The ID/IG ratio (0.3560) of PBGOCOF described the reduction and charge transformation between GO, COF, and PB nanocomposite. By using SEM the morphology of the composite was characterized and confirmed the formation of PBGOCOF composite. EMI shielding properties of the suggested material are investigated and a minimum SET value of −46 dB is obtained in all sample thicknesses. SER value is achieved at −46 dB. From the dielectric results, it is observed that the prepared sample has extraordinary properties of shielding absorbance which are useful for EMI Shielding.
doi_str_mv 10.1016/j.inoche.2022.109204
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The new age demands high thermal stability, lightweight, and strong absorptivity EM shielding materials with a broad absorption range of frequency band. The graphene oxide (GO) was synthesized through Hummer's method. Cobalt ferrite (COF) synthesized through the hydrothermal process and Prussian blue graphene oxide cobalt ferrite (PBGOCOF) synthesized through in-situ technique. The material formation confirmed through XRD and peaks are detected at 24.75°, 29.95°, 35.32°, 39.94°, 42.95°, 50.11°, 54.6°, 57.08° and 59.2° with corresponding crystal planes (111) (220) (311) (420) (422) (440) (600) (620) and (511) reflections. The epoxy, alkoxy, carboxyl, and O-H bonding was calculated through FTIR spectroscopy, and by using different bonding the material was characterized. Raman spectroscopy was used to analyze the chemical structure of the graphene and PBGOCOF. The ID/IG ratio (0.3560) of PBGOCOF described the reduction and charge transformation between GO, COF, and PB nanocomposite. By using SEM the morphology of the composite was characterized and confirmed the formation of PBGOCOF composite. EMI shielding properties of the suggested material are investigated and a minimum SET value of −46 dB is obtained in all sample thicknesses. SER value is achieved at −46 dB. 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The new age demands high thermal stability, lightweight, and strong absorptivity EM shielding materials with a broad absorption range of frequency band. The graphene oxide (GO) was synthesized through Hummer's method. Cobalt ferrite (COF) synthesized through the hydrothermal process and Prussian blue graphene oxide cobalt ferrite (PBGOCOF) synthesized through in-situ technique. The material formation confirmed through XRD and peaks are detected at 24.75°, 29.95°, 35.32°, 39.94°, 42.95°, 50.11°, 54.6°, 57.08° and 59.2° with corresponding crystal planes (111) (220) (311) (420) (422) (440) (600) (620) and (511) reflections. The epoxy, alkoxy, carboxyl, and O-H bonding was calculated through FTIR spectroscopy, and by using different bonding the material was characterized. Raman spectroscopy was used to analyze the chemical structure of the graphene and PBGOCOF. The ID/IG ratio (0.3560) of PBGOCOF described the reduction and charge transformation between GO, COF, and PB nanocomposite. By using SEM the morphology of the composite was characterized and confirmed the formation of PBGOCOF composite. EMI shielding properties of the suggested material are investigated and a minimum SET value of −46 dB is obtained in all sample thicknesses. SER value is achieved at −46 dB. 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The new age demands high thermal stability, lightweight, and strong absorptivity EM shielding materials with a broad absorption range of frequency band. The graphene oxide (GO) was synthesized through Hummer's method. Cobalt ferrite (COF) synthesized through the hydrothermal process and Prussian blue graphene oxide cobalt ferrite (PBGOCOF) synthesized through in-situ technique. The material formation confirmed through XRD and peaks are detected at 24.75°, 29.95°, 35.32°, 39.94°, 42.95°, 50.11°, 54.6°, 57.08° and 59.2° with corresponding crystal planes (111) (220) (311) (420) (422) (440) (600) (620) and (511) reflections. The epoxy, alkoxy, carboxyl, and O-H bonding was calculated through FTIR spectroscopy, and by using different bonding the material was characterized. Raman spectroscopy was used to analyze the chemical structure of the graphene and PBGOCOF. The ID/IG ratio (0.3560) of PBGOCOF described the reduction and charge transformation between GO, COF, and PB nanocomposite. By using SEM the morphology of the composite was characterized and confirmed the formation of PBGOCOF composite. EMI shielding properties of the suggested material are investigated and a minimum SET value of −46 dB is obtained in all sample thicknesses. SER value is achieved at −46 dB. From the dielectric results, it is observed that the prepared sample has extraordinary properties of shielding absorbance which are useful for EMI Shielding.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.inoche.2022.109204</doi></addata></record>
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subjects Dielectric study
EMI Shielding
Ferrites
Graphene
Magnetite
Nanocomposites
Prussian Blue
SEM
XRD Study
title Robust effectiveness behavior of synthesized cobalt doped Prussian blue graphene oxide ferrite against EMI shielding
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