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Effect of aging temperature on microstructure and mechanical properties of a novel Ti-6121 alloy

The effect of heat treatment on the microstructure and mechanical properties of a novel α + β Ti-6.2Al-0.8V-2.25Mo-1.2Cr-0.5Si (wt%) alloy was investigated in this paper. Microstructure and crystalline structure of the alloys after different solution and aging treatments were identified by scanning...

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Published in:Journal of alloys and compounds 2023-06, Vol.947, p.169612, Article 169612
Main Authors: Chen, Jianwei, Wang, Le, Fan, Qunbo, Sang, Zhuoyue, Xu, Yao, Wang, Changhao, Yao, Jiahao, Zhou, Zhiming, Yang, Liu, Liu, Zheng, Gao, Jinliang, Feng, Heyong
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cited_by cdi_FETCH-LOGICAL-c309t-e2666f9c6c42e6f3ae40b0eb54bf96683c379cda55e5f643a60458bce7dbbe5a3
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container_title Journal of alloys and compounds
container_volume 947
creator Chen, Jianwei
Wang, Le
Fan, Qunbo
Sang, Zhuoyue
Xu, Yao
Wang, Changhao
Yao, Jiahao
Zhou, Zhiming
Yang, Liu
Liu, Zheng
Gao, Jinliang
Feng, Heyong
description The effect of heat treatment on the microstructure and mechanical properties of a novel α + β Ti-6.2Al-0.8V-2.25Mo-1.2Cr-0.5Si (wt%) alloy was investigated in this paper. Microstructure and crystalline structure of the alloys after different solution and aging treatments were identified by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results indicated that a multi-scale microstructure was possessed in the heat-treated samples, which was composed of equiaxed primary α (αp) phase and nano-scale acicular secondary α (αs). After 900 ℃ solution for 1 h and 550 ℃ aging for 6 h, the alloy exhibited the optimal combination of strength and ductility (the ultimate tensile strength of ∼1387 MPa, the elongation of ∼11 %). Furthermore, the combination mechanism of strength-ductility of the sample under this condition was investigated. The samples before and after tensile fracture were analyzed using transmission electron microscope (TEM) and electron back-scattered diffraction (EBSD). The results showed that a large proportion of nano-scale acicular αs phases precipitated from the β matrix can effectively prevent the slip of dislocations and enhance the strength of the alloy. In addition, the multi-scale microstructure can create the strain partition, which can mediate the strain incompatibility between the αp and the transformed β (βT) to obtain an excellent combination of strength and ductility. •The heat-treated Ti-6121 alloy exhibits the ultimate tensile strength of ∼1387 MPa and the elongation of ∼11 %.•The ultrahigh tensile strength (1463 MPa) of Ti-6121 alloy should be mainly caused by the dense nano-scale acicular αs.•The outstanding combination of strength and ductility of Ti-6121 alloy should be attributed to the multi-scale microstructure.
doi_str_mv 10.1016/j.jallcom.2023.169612
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Microstructure and crystalline structure of the alloys after different solution and aging treatments were identified by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results indicated that a multi-scale microstructure was possessed in the heat-treated samples, which was composed of equiaxed primary α (αp) phase and nano-scale acicular secondary α (αs). After 900 ℃ solution for 1 h and 550 ℃ aging for 6 h, the alloy exhibited the optimal combination of strength and ductility (the ultimate tensile strength of ∼1387 MPa, the elongation of ∼11 %). Furthermore, the combination mechanism of strength-ductility of the sample under this condition was investigated. The samples before and after tensile fracture were analyzed using transmission electron microscope (TEM) and electron back-scattered diffraction (EBSD). 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Microstructure and crystalline structure of the alloys after different solution and aging treatments were identified by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results indicated that a multi-scale microstructure was possessed in the heat-treated samples, which was composed of equiaxed primary α (αp) phase and nano-scale acicular secondary α (αs). After 900 ℃ solution for 1 h and 550 ℃ aging for 6 h, the alloy exhibited the optimal combination of strength and ductility (the ultimate tensile strength of ∼1387 MPa, the elongation of ∼11 %). Furthermore, the combination mechanism of strength-ductility of the sample under this condition was investigated. The samples before and after tensile fracture were analyzed using transmission electron microscope (TEM) and electron back-scattered diffraction (EBSD). The results showed that a large proportion of nano-scale acicular αs phases precipitated from the β matrix can effectively prevent the slip of dislocations and enhance the strength of the alloy. In addition, the multi-scale microstructure can create the strain partition, which can mediate the strain incompatibility between the αp and the transformed β (βT) to obtain an excellent combination of strength and ductility. •The heat-treated Ti-6121 alloy exhibits the ultimate tensile strength of ∼1387 MPa and the elongation of ∼11 %.•The ultrahigh tensile strength (1463 MPa) of Ti-6121 alloy should be mainly caused by the dense nano-scale acicular αs.•The outstanding combination of strength and ductility of Ti-6121 alloy should be attributed to the multi-scale microstructure.</description><subject>Heat treatment</subject><subject>Microstructure evolution</subject><subject>Multi-scale microstructure</subject><subject>Strength-ductility combination</subject><subject>Tensile properties</subject><issn>0925-8388</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNqFkMtqwzAQRbVooWnaTyjoB-xKlqVYq1JC-oBAN-lalcejVMa2guQE8vd1HvuuBoa5dw6HkCfOcs64em7z1nYdhD4vWCFyrrTixQ2ZMV3IrBJVdUfuU2oZY1wLPiM_K-cQRhoctVs_bOmI_Q6jHfcRaRho7yGGNMY9nDd2aGiP8GsHD7ajuxim49FjOhfQIRywoxufTU85nUDC8YHcOtslfLzOOfl-W22WH9n66_1z-brOQDA9ZlgopZwGBWWBygmLJasZ1rKsnVaqEiAWGhorJUqnSmEVK2VVAy6aukZpxZzIS--JN0V0Zhd9b-PRcGZOakxrrmrMSY25qJlyL5ccTnAHj9Ek8DgANj5OYkwT_D8Nf7Jhcww</recordid><startdate>20230625</startdate><enddate>20230625</enddate><creator>Chen, Jianwei</creator><creator>Wang, Le</creator><creator>Fan, Qunbo</creator><creator>Sang, Zhuoyue</creator><creator>Xu, Yao</creator><creator>Wang, Changhao</creator><creator>Yao, Jiahao</creator><creator>Zhou, Zhiming</creator><creator>Yang, Liu</creator><creator>Liu, Zheng</creator><creator>Gao, Jinliang</creator><creator>Feng, Heyong</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230625</creationdate><title>Effect of aging temperature on microstructure and mechanical properties of a novel Ti-6121 alloy</title><author>Chen, Jianwei ; Wang, Le ; Fan, Qunbo ; Sang, Zhuoyue ; Xu, Yao ; Wang, Changhao ; Yao, Jiahao ; Zhou, Zhiming ; Yang, Liu ; Liu, Zheng ; Gao, Jinliang ; Feng, Heyong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c309t-e2666f9c6c42e6f3ae40b0eb54bf96683c379cda55e5f643a60458bce7dbbe5a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Heat treatment</topic><topic>Microstructure evolution</topic><topic>Multi-scale microstructure</topic><topic>Strength-ductility combination</topic><topic>Tensile properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chen, Jianwei</creatorcontrib><creatorcontrib>Wang, Le</creatorcontrib><creatorcontrib>Fan, Qunbo</creatorcontrib><creatorcontrib>Sang, Zhuoyue</creatorcontrib><creatorcontrib>Xu, Yao</creatorcontrib><creatorcontrib>Wang, Changhao</creatorcontrib><creatorcontrib>Yao, Jiahao</creatorcontrib><creatorcontrib>Zhou, Zhiming</creatorcontrib><creatorcontrib>Yang, Liu</creatorcontrib><creatorcontrib>Liu, Zheng</creatorcontrib><creatorcontrib>Gao, Jinliang</creatorcontrib><creatorcontrib>Feng, Heyong</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chen, Jianwei</au><au>Wang, Le</au><au>Fan, Qunbo</au><au>Sang, Zhuoyue</au><au>Xu, Yao</au><au>Wang, Changhao</au><au>Yao, Jiahao</au><au>Zhou, Zhiming</au><au>Yang, Liu</au><au>Liu, Zheng</au><au>Gao, Jinliang</au><au>Feng, Heyong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of aging temperature on microstructure and mechanical properties of a novel Ti-6121 alloy</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2023-06-25</date><risdate>2023</risdate><volume>947</volume><spage>169612</spage><pages>169612-</pages><artnum>169612</artnum><issn>0925-8388</issn><abstract>The effect of heat treatment on the microstructure and mechanical properties of a novel α + β Ti-6.2Al-0.8V-2.25Mo-1.2Cr-0.5Si (wt%) alloy was investigated in this paper. Microstructure and crystalline structure of the alloys after different solution and aging treatments were identified by scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results indicated that a multi-scale microstructure was possessed in the heat-treated samples, which was composed of equiaxed primary α (αp) phase and nano-scale acicular secondary α (αs). After 900 ℃ solution for 1 h and 550 ℃ aging for 6 h, the alloy exhibited the optimal combination of strength and ductility (the ultimate tensile strength of ∼1387 MPa, the elongation of ∼11 %). Furthermore, the combination mechanism of strength-ductility of the sample under this condition was investigated. The samples before and after tensile fracture were analyzed using transmission electron microscope (TEM) and electron back-scattered diffraction (EBSD). The results showed that a large proportion of nano-scale acicular αs phases precipitated from the β matrix can effectively prevent the slip of dislocations and enhance the strength of the alloy. In addition, the multi-scale microstructure can create the strain partition, which can mediate the strain incompatibility between the αp and the transformed β (βT) to obtain an excellent combination of strength and ductility. •The heat-treated Ti-6121 alloy exhibits the ultimate tensile strength of ∼1387 MPa and the elongation of ∼11 %.•The ultrahigh tensile strength (1463 MPa) of Ti-6121 alloy should be mainly caused by the dense nano-scale acicular αs.•The outstanding combination of strength and ductility of Ti-6121 alloy should be attributed to the multi-scale microstructure.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2023.169612</doi></addata></record>
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subjects Heat treatment
Microstructure evolution
Multi-scale microstructure
Strength-ductility combination
Tensile properties
title Effect of aging temperature on microstructure and mechanical properties of a novel Ti-6121 alloy
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