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Texture tailoring and microstructure refinement induced by {11−21} and {10−12} twinning in an extruded Mg-Gd alloy

An extruded Mg-17Gd (wt%) alloy with  fiber texture was compressed along different directions at room temperature. Electron backscatter diffraction characterization was used to investigate the texture tailoring, twinning and dynamic recrystallization (DRX) behaviors. The results indicate that {10−12...

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Published in:Journal of alloys and compounds 2023-12, Vol.966, p.171590, Article 171590
Main Authors: Lv, Ning, Zhao, Lingyu, Yan, Hong, Liu, Boyu, Mao, Yaozong, Shan, Zhiwei, Chen, Rongshi
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container_title Journal of alloys and compounds
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Zhao, Lingyu
Yan, Hong
Liu, Boyu
Mao, Yaozong
Shan, Zhiwei
Chen, Rongshi
description An extruded Mg-17Gd (wt%) alloy with  fiber texture was compressed along different directions at room temperature. Electron backscatter diffraction characterization was used to investigate the texture tailoring, twinning and dynamic recrystallization (DRX) behaviors. The results indicate that {10−12} and {11−21} twinning activated. The [0001] pole tilted to compression direction with the strain increasing and twinning dominated the texture transition. Activation of {10−12} twinning can be governed by Schmid law, while it is more appropriate to explain the activation of {11−21} twinning by the basal slip transfer condition in the twinned grains according to the slip trace analysis. In addition, operation of {11−21} twinning can facilitate the nucleation of {10−12} twin in the same grain by changing Schmid factor (SF) in the vicinities of {11−21} twin. Grain refinement occurred in the specimens with large strain and the average grain size decrease from ∼27 µm to ∼12 µm. The mechanism of grain refinement can be summarized as follows: the mobility of twin boundaries will be restricted because of the twin-twin and dislocation-twin interaction and converted to random high angle grain boundaries (HAGBs). The random HAGBs offer the nucleation sites and the strain accumulation within twins offer the driving force which facilitate the formation of DRXed grains at random HAGBs. Additionally, the SF difference within parent grain may result in the formation of HAGBs, and these HAGBs can connected the random HAGBs that result from the dislocation-twin interaction which result in the formation of new grains. •{11-21} twinning behavior in Mg alloys with [0001] fiber texture was firstly investigated.•Interaction between twins and the influence of twinning on microstructure evolution were systematically investigated.•Dynamic recrystallization induced by {11-21} twinning was observed.•Twin-twin and dislocation-twin interaction facilitated the microstructure refinement.
doi_str_mv 10.1016/j.jallcom.2023.171590
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Electron backscatter diffraction characterization was used to investigate the texture tailoring, twinning and dynamic recrystallization (DRX) behaviors. The results indicate that {10−12} and {11−21} twinning activated. The [0001] pole tilted to compression direction with the strain increasing and twinning dominated the texture transition. Activation of {10−12} twinning can be governed by Schmid law, while it is more appropriate to explain the activation of {11−21} twinning by the basal slip transfer condition in the twinned grains according to the slip trace analysis. In addition, operation of {11−21} twinning can facilitate the nucleation of {10−12} twin in the same grain by changing Schmid factor (SF) in the vicinities of {11−21} twin. Grain refinement occurred in the specimens with large strain and the average grain size decrease from ∼27 µm to ∼12 µm. 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Electron backscatter diffraction characterization was used to investigate the texture tailoring, twinning and dynamic recrystallization (DRX) behaviors. The results indicate that {10−12} and {11−21} twinning activated. The [0001] pole tilted to compression direction with the strain increasing and twinning dominated the texture transition. Activation of {10−12} twinning can be governed by Schmid law, while it is more appropriate to explain the activation of {11−21} twinning by the basal slip transfer condition in the twinned grains according to the slip trace analysis. In addition, operation of {11−21} twinning can facilitate the nucleation of {10−12} twin in the same grain by changing Schmid factor (SF) in the vicinities of {11−21} twin. Grain refinement occurred in the specimens with large strain and the average grain size decrease from ∼27 µm to ∼12 µm. The mechanism of grain refinement can be summarized as follows: the mobility of twin boundaries will be restricted because of the twin-twin and dislocation-twin interaction and converted to random high angle grain boundaries (HAGBs). The random HAGBs offer the nucleation sites and the strain accumulation within twins offer the driving force which facilitate the formation of DRXed grains at random HAGBs. Additionally, the SF difference within parent grain may result in the formation of HAGBs, and these HAGBs can connected the random HAGBs that result from the dislocation-twin interaction which result in the formation of new grains. •{11-21} twinning behavior in Mg alloys with [0001] fiber texture was firstly investigated.•Interaction between twins and the influence of twinning on microstructure evolution were systematically investigated.•Dynamic recrystallization induced by {11-21} twinning was observed.•Twin-twin and dislocation-twin interaction facilitated the microstructure refinement.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2023.171590</doi><orcidid>https://orcid.org/0000-0003-1222-2201</orcidid><orcidid>https://orcid.org/0000-0003-4641-3401</orcidid></addata></record>
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subjects Grain refinement
Magnesium alloy
Slip traces analysis
Texture
{11−21} twinning
title Texture tailoring and microstructure refinement induced by {11−21} and {10−12} twinning in an extruded Mg-Gd alloy
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