Synthesis and characterization of some mixed ligands complexes of β-enaminone with some metal ions

The study includes the perpetration and characterization of new ligand of β-enaminone with its mixed ligands complexes of first transition element ions which their formula are [(M)(L1)(8.h.q)]; M = [Co(II), Ni(II), Cu(II), Zn(II) and Cd(II)]. The prepared ligand and its complexes were diagnosed by t...

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Bibliographic Details
Published in:Materials today : proceedings 2023, Vol.80, p.1683-1690
Main Authors: Abdul-Sattar Mohamed, Fatimah, Numan, Ahmed T.
Format: Article
Language:English
Subjects:
Complexes
Enaminone
First transition elements
Hydroxy quinoline
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Summary:The study includes the perpetration and characterization of new ligand of β-enaminone with its mixed ligands complexes of first transition element ions which their formula are [(M)(L1)(8.h.q)]; M = [Co(II), Ni(II), Cu(II), Zn(II) and Cd(II)]. The prepared ligand and its complexes were diagnosed by the (FT-IR) furrier transform infrared spectroscopy, (Uv–vis) ultraviolete-visible spectroscopy, (1H-, 13C NMR Nuclear magnetic resonance spectroscopy or Resonanse), mass spectroscopy, melting point, thin film chromatography on thin layer chromatoraphy, and (CHNS) analysis. The results prove that the ligand behave as bidentate chelating through the exocyclic oxygen and nitrogen atoms.“
ISSN:2214-7853
2214-7853
DOI:10.1016/j.matpr.2023.02.317