Trans-etherification of catechol-type benzylic ether with diols as a route to new sterically hindered bis-catechols

[Display omitted] The trans-etherification of 4,6-di-tert-butyl-2,3-dihydroxybenzyl methyl ether with α,ω-alkanediols under mild conditions (CHCl3, 65°C) leads to new sterically hindered biscatechols in high yields. The molecular structures of three of them was determined by single-crystal X-ray dif...

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Published in:Mendeleev communications 2019-01, Vol.29 (1), p.91-93
Main Authors: Zhiganshina, Elnara R., Arsenyev, Maxim V., Shavyrin, Andrey S., Baranov, Evgeny V., Chesnokov, Sergey A.
Format: Article
Language:English
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Summary:[Display omitted] The trans-etherification of 4,6-di-tert-butyl-2,3-dihydroxybenzyl methyl ether with α,ω-alkanediols under mild conditions (CHCl3, 65°C) leads to new sterically hindered biscatechols in high yields. The molecular structures of three of them was determined by single-crystal X-ray diffraction.
ISSN:0959-9436
DOI:10.1016/j.mencom.2019.01.031