Hydrolytic polycondensation of trimethoxymethylsilane under ultrasonic irradiation

[Display omitted] The hydrolytic polycondensation of trimethoxymethylsilane in the absence of catalyst and solvent under ultrasonic irradiation was performed, the effect of reagent ratio, power, temperature and irradiation duration on the process outcome was estimated. Thus obtained polyorganosilses...

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Bibliographic Details
Published in:Mendeleev communications 2020-05, Vol.30 (3), p.336-338
Main Authors: Yakhontov, Nikita G., Gorbatsevich, Olga B., Kalinina, Alexandra A., Demchenko, Nina V., Kazakova, Valentina V., Muzafarov, Aziz M.
Format: Article
Language:English
Subjects:
alkoxysilanes
hydrolytic polycondensation
polyorganosilsesquioxanes
trimethoxymethylsilane
ultrasonic irradiation
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Summary:[Display omitted] The hydrolytic polycondensation of trimethoxymethylsilane in the absence of catalyst and solvent under ultrasonic irradiation was performed, the effect of reagent ratio, power, temperature and irradiation duration on the process outcome was estimated. Thus obtained polyorganosilsesquioxanes were characterized by 1H NMR and IR spectroscopy as well as gel permeation chromatography.
ISSN:0959-9436
DOI:10.1016/j.mencom.2020.05.025