Microstructural modification and its effect on strengthening mechanism and yield asymmetry of in-situ TiC-TiB2/ AZ91 magnesium matrix composite

• Published in: Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2018-05, Vol.724, p.269-282
• Main Authors: Sahoo, B.N., MD, F. Khan, Babu, S., Panigrahi, S.K., Janaki Ram, G.D.
• Format: Article
• Language: English
• Subjects: Friction stir processing; In-situ magnesium matrix composite; Microstructural properties; Strengthening mechanism; Tension-compression yield asymmetry
• ISSN: 0921-5093; 1873-4936
• DOI: 10.1016/j.msea.2018.03.060

The application of AZ91 magnesium alloy is limited because of dendritic β-Mg17Al12 phase which degrades mechanical properties and causes high tension to compression yield asymmetry (R). To overcome this, a severe plastic deformation (SPD) based hybrid process has been implemented in this study, to develop in-situ AZ91 + TiC-TiB2 composite. This results in redistribution of β-Mg17Al12 phase on the grain boundaries along with notable grain refinement. The combined effect of in-situ reinforcement and grain refinement due to SPD process resulted in simultaneous enhancement of strength and ductility. Further, intense grain refinement and presence of TiC-TiB2 reinforcement in the grain boundary region is found to increase the stress concentration along the grain boundary which hinders twin nucleation and significantly reduces the R value from 1.42 (as-cast condition) to 1.04 (SPDed in-situ composite). The underlying mechanism of significant property enhancement in the developed material has been correlated with the tension and compression tests and microstructures.