Conditional optimisation of wet chemical synthesis for pioneered ZnO nanostructures

A protocol for novel Zinc oxide nano-geometry has been developed through conditional (pH, solvent and temperature) optimisation of simple wet chemical based acidic route synthesis. A monodispersed needle-topped nanorod and nanorosette structures pioneered for technological devices are prepared. Poss...

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Bibliographic Details
Published in:Nano-Structures & Nano-Objects 2017-02, Vol.9, p.26-30
Main Authors: Das, Debadrito, Datta, Animesh Kumar, Kumbhakar, Divya Vishambhar, Ghosh, Bapi, Pramanik, Ankita, Gupta, Sudha
Format: Article
Language:English
Subjects:
Conditional optimisation
Nanorosette
Needle-topped nanorod
Wet chemical synthesis
ZnO nanostructures
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Summary:A protocol for novel Zinc oxide nano-geometry has been developed through conditional (pH, solvent and temperature) optimisation of simple wet chemical based acidic route synthesis. A monodispersed needle-topped nanorod and nanorosette structures pioneered for technological devices are prepared. Possible reaction kinetics is proposed for the nanostructural growth. Prepared nanocrystals are opto-physically characterised using UV–visible spectroscopy, Fourier transform infra-red spectroscopy, X-ray diffraction, Dynamic light scattering-zeta potential and Field emission scanning electron microscopy. [Display omitted]
ISSN:2352-507X
DOI:10.1016/j.nanoso.2016.12.002