Large scale synthesis of acetylene dicarboxaldehyde mono and diacetal

An easy, high yield, large scale, and atom economical, synthesis of the valuable acetylene dicarboxaldehyde dimethyl and tetramethyl acetals was described starting from 2,5-dimethoxy-2,5-furan. An easy, high yield, large scale, and atom economical, synthesis of the valuable acetylene dicarboxaldehyd...

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Bibliographic Details
Published in:Tetrahedron letters 2004-02, Vol.45 (9), p.1829-1832
Main Authors: Akué-Gédu, Rufine, Rigo, Benoı̂t
Format: Article
Language:English
Subjects:
2,5-Dimethoxy-2,5-dihydrofuran
Acetylene dicarboxaldehyde
Atom economy
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Summary:An easy, high yield, large scale, and atom economical, synthesis of the valuable acetylene dicarboxaldehyde dimethyl and tetramethyl acetals was described starting from 2,5-dimethoxy-2,5-furan. An easy, high yield, large scale, and atom economical, synthesis of the valuable acetylene dicarboxaldehyde dimethyl and tetramethyl acetals was described starting from 2,5-dimethoxy-2,5-furan.
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2004.01.022