One-pot synthesis of cyclic enecarbamates from lactam carbamates

[Display omitted] A general, practical and efficient one-pot synthesis of cyclic enecarbamates is described. The protocol proceeds via reduction of lactam carbamate with Super-Hydride ®, followed by in situ dehydration with trifluoroacetic anhydride (TFAA) and diisopropylethylamine (DIPEA).

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Bibliographic Details
Published in:Tetrahedron letters 2005-06, Vol.46 (23), p.4011-4013
Main Authors: Yu, Jurong, Truc, Vu, Riebel, Peter, Hierl, Elizabeth, Mudryk, Boguslaw
Format: Article
Language:English
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Summary:[Display omitted] A general, practical and efficient one-pot synthesis of cyclic enecarbamates is described. The protocol proceeds via reduction of lactam carbamate with Super-Hydride ®, followed by in situ dehydration with trifluoroacetic anhydride (TFAA) and diisopropylethylamine (DIPEA).
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2005.04.030