Synthesis of thiol-capped gold nanoparticle with a flow system using organosilane as a reducing agent

Synthesis of thiol-capped gold nanoparticle is carried out by mixing of a THF solution of HAuCl4·4H2O and nC12H25SH with a THF solution of triethylsilane in a flow system that consists of polytetrafluoroethylene tubing. The effect of residence time and reaction temperature on the particle size is ex...

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Bibliographic Details
Published in:Tetrahedron letters 2012-08, Vol.53 (33), p.4457-4459
Main Authors: Sugie, Atsushi, Song, Hansoo, Horie, Takafumi, Ohmura, Naoto, Kanie, Kiyoshi, Muramatsu, Atsushi, Mori, Atsunori
Format: Article
Language:English
Subjects:
Alkanethiol
Flow reactor
Gold nanoparticle
THP thioether
Triethylsilane
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Summary:Synthesis of thiol-capped gold nanoparticle is carried out by mixing of a THF solution of HAuCl4·4H2O and nC12H25SH with a THF solution of triethylsilane in a flow system that consists of polytetrafluoroethylene tubing. The effect of residence time and reaction temperature on the particle size is examined.
ISSN:0040-4039
1873-3581
DOI:10.1016/j.tetlet.2012.06.056