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One-pot solvent-free reductive amination with a solid ammonium carbamate salt from CO 2 and amine
Many amines are liquid and their handling is inconvenient compared with the corresponding solids. We transformed a liquid ( S )-(−)-1-phenylethylamine 1 to the corresponding neutral solid form 2 by reacting with carbon dioxide. We performed reductive amination of 2 with various aldehydes 3 under sol...
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| Published in: | RSC advances 2014, Vol.4 (86), p.46203-46207 |
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| Main Authors: | , , , , , , |
| Format: | Article |
| Language: | English |
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| cited_by | cdi_FETCH-LOGICAL-c76G-4984b3736dbc3be081bd607a8406ee7fa905ddb79d9edbc9f2b86fd94c08374a3 |
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| cites | cdi_FETCH-LOGICAL-c76G-4984b3736dbc3be081bd607a8406ee7fa905ddb79d9edbc9f2b86fd94c08374a3 |
| container_end_page | 46207 |
| container_issue | 86 |
| container_start_page | 46203 |
| container_title | RSC advances |
| container_volume | 4 |
| creator | Kang, Philjun Lee, Kyu Myung Lee, Won Koo Lee, Kyu Hyung Lee, Byeongno Cho, Jaeheung Hur, Nam Hwi |
| description | Many amines are liquid and their handling is inconvenient compared with the corresponding solids. We transformed a liquid (
S
)-(−)-1-phenylethylamine
1
to the corresponding neutral solid form
2
by reacting with carbon dioxide. We performed reductive amination of
2
with various aldehydes
3
under solvent-free conditions to provide secondary amines
5
in high yields. |
| doi_str_mv | 10.1039/C4RA07558G |
| format | article |
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S
)-(−)-1-phenylethylamine
1
to the corresponding neutral solid form
2
by reacting with carbon dioxide. We performed reductive amination of
2
with various aldehydes
3
under solvent-free conditions to provide secondary amines
5
in high yields.</description><identifier>ISSN: 2046-2069</identifier><identifier>EISSN: 2046-2069</identifier><identifier>DOI: 10.1039/C4RA07558G</identifier><language>eng</language><ispartof>RSC advances, 2014, Vol.4 (86), p.46203-46207</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c76G-4984b3736dbc3be081bd607a8406ee7fa905ddb79d9edbc9f2b86fd94c08374a3</citedby><cites>FETCH-LOGICAL-c76G-4984b3736dbc3be081bd607a8406ee7fa905ddb79d9edbc9f2b86fd94c08374a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,4009,27902,27903,27904</link.rule.ids></links><search><creatorcontrib>Kang, Philjun</creatorcontrib><creatorcontrib>Lee, Kyu Myung</creatorcontrib><creatorcontrib>Lee, Won Koo</creatorcontrib><creatorcontrib>Lee, Kyu Hyung</creatorcontrib><creatorcontrib>Lee, Byeongno</creatorcontrib><creatorcontrib>Cho, Jaeheung</creatorcontrib><creatorcontrib>Hur, Nam Hwi</creatorcontrib><title>One-pot solvent-free reductive amination with a solid ammonium carbamate salt from CO 2 and amine</title><title>RSC advances</title><description>Many amines are liquid and their handling is inconvenient compared with the corresponding solids. We transformed a liquid (
S
)-(−)-1-phenylethylamine
1
to the corresponding neutral solid form
2
by reacting with carbon dioxide. We performed reductive amination of
2
with various aldehydes
3
under solvent-free conditions to provide secondary amines
5
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S
)-(−)-1-phenylethylamine
1
to the corresponding neutral solid form
2
by reacting with carbon dioxide. We performed reductive amination of
2
with various aldehydes
3
under solvent-free conditions to provide secondary amines
5
in high yields.</abstract><doi>10.1039/C4RA07558G</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2046-2069 |
| ispartof | RSC advances, 2014, Vol.4 (86), p.46203-46207 |
| issn | 2046-2069 2046-2069 |
| language | eng |
| recordid | cdi_crossref_primary_10_1039_C4RA07558G |
| source | Royal Society of Chemistry:Jisc Collections:Royal Society of Chemistry Read and Publish 2022-2024 (reading list) |
| title | One-pot solvent-free reductive amination with a solid ammonium carbamate salt from CO 2 and amine |
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