Pulsed EPR spectrometer

A pulsed EPR spectrometer is described. This spectrometer is designed for the study of relaxation times of dilute solutions of samples in common solvents as a function of temperature both above and below room temperature. Resolution of pulse widths and spacings is 1 ns. Both continuous wave (cw) and...

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Bibliographic Details
Published in:Review of scientific instruments 1987-09, Vol.58 (9), p.1709-1723
Main Authors: Quine, Richard W., Eaton, Gareth R., Eaton, Sandra S.
Format: Article
Language:English
Subjects:
Exact sciences and technology
Infrared, submillimeter wave, microwave and radiowave instruments, equipment and techniques
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Physics
Submillimeter wave, microwave and radiowave spectrometers
magnetic resonance spectrometers, auxiliary equipments and techniques
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Summary:A pulsed EPR spectrometer is described. This spectrometer is designed for the study of relaxation times of dilute solutions of samples in common solvents as a function of temperature both above and below room temperature. Resolution of pulse widths and spacings is 1 ns. Both continuous wave (cw) and pulsed electron spin‐echo studies can be done on the same sample on the same spectrometer. Details of component choices and timing synchronization are provided. Phase alternation sequences for eliminating unwanted echoes are described. Examples of performance of the spectrometer are presented.
ISSN:0034-6748
1089-7623
DOI:10.1063/1.1139373