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One-pot synthesis of 4,4′-diamino-3,3′-bifurazan

The title compound 1 has been synthesized by a one-pot procedure starting from 3,4-di(hydroximinomethyl)furoxan 7 and hydroxylamine, with pH increasing over the course of the reaction from 1 to 10.

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Bibliographic Details
Published in:Mendeleev communications 1996, Vol.6 (6), p.246-247
Main Authors: Sheremetev, Aleksei B., Mantseva, Elena V.
Format: Article
Language:English
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Description
Summary:The title compound 1 has been synthesized by a one-pot procedure starting from 3,4-di(hydroximinomethyl)furoxan 7 and hydroxylamine, with pH increasing over the course of the reaction from 1 to 10.
ISSN:0959-9436
DOI:10.1070/MC1996v006n06ABEH000745