Non-Isothermal Crystallization Kinetics of Polyamide 6/h-Boron Nitride Composites

Hexagonal boron nitride nanosheets were mixed with polyamide 6 to fabricate polymer-based composites by using a solution blending method. The nonisothermal crystallization behaviors of the as-prepared composites were investigated via differential scanning calorimetry. Results showed that the peak te...

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Published in:Journal of macromolecular science. Physics 2017-03, Vol.56 (3), p.170-177
Main Authors: Wu, Xiang-Feng, Zhao, Yong-Ke, Li, Hui, Zhao, Ze-Hua, Sun, Yang, Zhang, Han, Yu, Mai-Tuo, Jia, Fan-Fan
Format: Article
Language:English
Subjects:
Alloys
Boron
Boron nitride
Calorimetry
Cooling
Cooling curves
Cooling rate
Crystallization
Differential scanning calorimetry
Fillers
Heat measurement
Heat treating
hexagonal boron nitride
Kinetics
Nanostructure
non-isothermal crystallization
polyamide 6
Polyamide resins
Polyamides
Polymer matrix composites
Solution blending
Temperature effects
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cited_by cdi_FETCH-LOGICAL-c371t-4fdb2b648ccbc17ac8a00e554c03dd8781176d83c1565eec45f1e0f8db0940a23
cites cdi_FETCH-LOGICAL-c371t-4fdb2b648ccbc17ac8a00e554c03dd8781176d83c1565eec45f1e0f8db0940a23
container_end_page 177
container_issue 3
container_start_page 170
container_title Journal of macromolecular science. Physics
container_volume 56
creator Wu, Xiang-Feng
Zhao, Yong-Ke
Li, Hui
Zhao, Ze-Hua
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Zhang, Han
Yu, Mai-Tuo
Jia, Fan-Fan
description Hexagonal boron nitride nanosheets were mixed with polyamide 6 to fabricate polymer-based composites by using a solution blending method. The nonisothermal crystallization behaviors of the as-prepared composites were investigated via differential scanning calorimetry. Results showed that the peak temperature of the exothermic crystallization curve was moved to lower temperature with increase in the cooling rate. At the same cooling rate, the peak temperature of the pure polyamide 6 was lower than those of the composites. Moreover, the crystallization rate increased gradually with increase in the cooling rate. In addition, at the cooling rates of 5 or 10°C min −1 , the crystallization rate of pure polyamide 6 was higher than those of all compositions of the composites. However, at the cooling rates of 20 or 40°C min −1 , the crystallization rate decreased first and then increased with increase in the fillers loading. The crystallization mechanism was between one-dimensional and two-dimensional during the crystallization process.
doi_str_mv 10.1080/00222348.2017.1280719
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The nonisothermal crystallization behaviors of the as-prepared composites were investigated via differential scanning calorimetry. Results showed that the peak temperature of the exothermic crystallization curve was moved to lower temperature with increase in the cooling rate. At the same cooling rate, the peak temperature of the pure polyamide 6 was lower than those of the composites. Moreover, the crystallization rate increased gradually with increase in the cooling rate. In addition, at the cooling rates of 5 or 10°C min −1 , the crystallization rate of pure polyamide 6 was higher than those of all compositions of the composites. However, at the cooling rates of 20 or 40°C min −1 , the crystallization rate decreased first and then increased with increase in the fillers loading. The crystallization mechanism was between one-dimensional and two-dimensional during the crystallization process.</description><identifier>ISSN: 0022-2348</identifier><identifier>EISSN: 1525-609X</identifier><identifier>DOI: 10.1080/00222348.2017.1280719</identifier><language>eng</language><publisher>New York: Taylor &amp; Francis</publisher><subject>Alloys ; Boron ; Boron nitride ; Calorimetry ; Cooling ; Cooling curves ; Cooling rate ; Crystallization ; Differential scanning calorimetry ; Fillers ; Heat measurement ; Heat treating ; hexagonal boron nitride ; Kinetics ; Nanostructure ; non-isothermal crystallization ; polyamide 6 ; Polyamide resins ; Polyamides ; Polymer matrix composites ; Solution blending ; Temperature effects</subject><ispartof>Journal of macromolecular science. 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subjects Alloys
Boron
Boron nitride
Calorimetry
Cooling
Cooling curves
Cooling rate
Crystallization
Differential scanning calorimetry
Fillers
Heat measurement
Heat treating
hexagonal boron nitride
Kinetics
Nanostructure
non-isothermal crystallization
polyamide 6
Polyamide resins
Polyamides
Polymer matrix composites
Solution blending
Temperature effects
title Non-Isothermal Crystallization Kinetics of Polyamide 6/h-Boron Nitride Composites
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