Ultrasound-Assisted Synthesis of β-Enaminonitriles in the Presence of Base

Application of ultrasound shows significant rate enhancement for the synthesis of β-enaminonitriles in the presence of base. The role of various homogeneous and heterogeneous bases/solvents was also studied for the reaction, and potassium t-butoxide/t-butyl alcohol combination was found to give the...

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Bibliographic Details
Published in:Synthetic communications 2007-07, Vol.37 (13), p.2253-2258
Main Authors: Jagtap, Sachin R., Bhanushali, Mayur J., Nandurkar, Nitin S., Bhanage, Bhalchandra M.
Format: Article
Language:English
Subjects:
potassium t-butoxide
t-butyl alcohol
ultrasound
β-enaminonitriles
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Summary:Application of ultrasound shows significant rate enhancement for the synthesis of β-enaminonitriles in the presence of base. The role of various homogeneous and heterogeneous bases/solvents was also studied for the reaction, and potassium t-butoxide/t-butyl alcohol combination was found to give the best result at room temperature.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397910701397144