Access to New Reactive Unsaturated Cycloalkenethiones by Flash Vacuum Thermolysis

The reactive conjugated cycloalkenethiones (3, 4, 5) have been synthesized from the corresponding cycloalkenylsulfanyl compounds under flash vacuum thermolysis (FVT) conditions. The nonconjugated cycloalkenethiones (8, 9) were prepared in the same way, the tautomerisation into cycloalkadienethiols (...

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Published in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 1999-01, Vol.153 (1), p.387-388
Main Authors: Briard, Emmanuelle, Levillain, Jocelyne, Ripoll, Jean-Louis
Format: Article
Language:English
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cycloalkenethione
flash vacuum thermolysis
retro-ene
vinylthioketene
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container_title Phosphorus, sulfur, and silicon and the related elements
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creator Briard, Emmanuelle
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Ripoll, Jean-Louis
description The reactive conjugated cycloalkenethiones (3, 4, 5) have been synthesized from the corresponding cycloalkenylsulfanyl compounds under flash vacuum thermolysis (FVT) conditions. The nonconjugated cycloalkenethiones (8, 9) were prepared in the same way, the tautomerisation into cycloalkadienethiols (10, 11) occurred at 77 K. As for the cyclobutenethione 13, only the ring opening products were observed at 77 K.
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subjects cycloalkenethione
flash vacuum thermolysis
retro-ene
vinylthioketene
title Access to New Reactive Unsaturated Cycloalkenethiones by Flash Vacuum Thermolysis
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