Identification and Quantitative Determination of Madder by High Performance Liquid Chromatography: Application to Historical Textiles

A reversed phase HPLC method has been developed for the identification and quantification of madder applied to an old textile. An isocratic method was used for the identification of alizarin and purpurin, the main pigments in the madder plant, which were identified and quantified in cotton and wool...

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Bibliographic Details
Published in:Journal of liquid chromatography & related technologies 2009-09, Vol.32 (16), p.2334-2345
Main Authors: Zarkogianni, M., Papliaka, Z.-E., Tsatsaroni, E.
Format: Article
Language:English
Subjects:
Alizarin
Analytical chemistry
Applied sciences
Chemistry
Chromatographic methods and physical methods associated with chromatography
Exact sciences and technology
Fibers and threads
Forms of application and semi-finished materials
FT-IR spectroscopy
Isocratic HPLC
Madder
Other chromatographic methods
Polymer industry, paints, wood
Purpurin
Technology of polymers
Textile
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Summary:A reversed phase HPLC method has been developed for the identification and quantification of madder applied to an old textile. An isocratic method was used for the identification of alizarin and purpurin, the main pigments in the madder plant, which were identified and quantified in cotton and wool reference samples and in the unknown textile. FTIR-spectroscopy was also used for the identification of pigment and fiber of the unknown sample.
ISSN:1082-6076
1520-572X
DOI:10.1080/10826070903187874