Synthesis, Identification, and Solubility of Adducts of Aldonitrones to Light Fullerenes in Toluene and O-xylene

In this paper, a synthesis of the four adducts of aldonitrones to light fullerenes (C 60 and C 70 ) is described. Identifications of adducts were conducted using infrared and electron spectroscopy and nuclear magnetic resonance, elemental analysis, and mass-spectrometry method. In the temperature ra...

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Bibliographic Details
Published in:Fullerenes, nanotubes, and carbon nanostructures nanotubes, and carbon nanostructures, 2015-04, Vol.23 (4), p.355-360
Main Authors: Kritchenkov, Andreii S., Semenov, Konstantin N., Charykov, Nikolai A.
Format: Article
Language:English
Subjects:
aldonitrones
fullerenes
solubility
thermogravimetric analysis
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Summary:In this paper, a synthesis of the four adducts of aldonitrones to light fullerenes (C 60 and C 70 ) is described. Identifications of adducts were conducted using infrared and electron spectroscopy and nuclear magnetic resonance, elemental analysis, and mass-spectrometry method. In the temperature range 20-80°С we studied the dependences of solubility of these adducts in aromatic solvents-toluene and o-xylene.
ISSN:1536-383X
1536-4046
DOI:10.1080/1536383X.2014.913576