Trichloroisocynuric Acid/DMF as Efficient Reagent for Chlorodehydration of Alcohols Under Conventional and Ultrasonic Conditions

A new and efficient method for the chlorodehydration of alcohols utilizing TCCA/DMF is described. Various alcohols can be converted smoothly into their corresponding alkyl chlorides in high yields under mild conditions with short reaction times.

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Bibliographic Details
Published in:Inorganic and nano-metal chemistry 2015-01, Vol.45 (1), p.97-103
Main Authors: Venkanna, Purugula, Kumar, Mukka Satish, Rajanna, Kamatala Chinna, Ali, Mir Moazzam
Format: Article
Language:English
Subjects:
Alcohols
alkyl chlorides
chlorodehydration
N dimethyl formamide
Reagents
sonication
trichloroisocyanuric acid
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Description
Summary:A new and efficient method for the chlorodehydration of alcohols utilizing TCCA/DMF is described. Various alcohols can be converted smoothly into their corresponding alkyl chlorides in high yields under mild conditions with short reaction times.
ISSN:1553-3174
2470-1556
1553-3182
2470-1564
DOI:10.1080/15533174.2013.819896