The Sulphides, Sulfoxides, and Sulfones of New Dienyl Groups

Mono(thio)substituted dienes 1a-c gave compounds 3a-i with piperazine 2 in dichloromethane. Compounds 5a-c were synthesized from the reaction of mono(thio)substituted 1a-c with 4-piperidinol 4 . Compounds 7a-b were obtained from the reaction of mono(thio)substituted dienes 1a-b with 2-aminoethylmorp...

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Bibliographic Details
Published in:Phosphorus, sulfur, and silicon and the related elements sulfur, and silicon and the related elements, 2003-10, Vol.178 (10), p.2297-2305
Main Authors: İbiş, Cemil, Gökmen, Zeliha
Format: Article
Language:English
Subjects:
Hexachlorobutadiene
Mono(thio)- And Di(thio)-substituted Halodienes
N,S-thiosubstituted Nitrodiene
Piperazine
Piperidine
Sulfone
Sulfoxide
Thioether
Thiol
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Summary:Mono(thio)substituted dienes 1a-c gave compounds 3a-i with piperazine 2 in dichloromethane. Compounds 5a-c were synthesized from the reaction of mono(thio)substituted 1a-c with 4-piperidinol 4 . Compounds 7a-b were obtained from the reaction of mono(thio)substituted dienes 1a-b with 2-aminoethylmorpholino 6 . N,N-Bis(mono(thio)substituted)-2-nitro-1,3-butadienyl 9a-b were synthesized from the reactions of mono(thio)substituted dienes 1a-b with 2,5-dimethyl-piperazine 8 . Compound 10a was obtained from the reaction of perchlorobutadiene with 2-napthylthiol in ethanol in the presence of sodium hydroxide. Compounds 11a-b were obtained from the reactions of mono(thio)substituted dienes 10a-b with m-chloroperbenzoic acid in CHCl 3 . Di(thio)substituted diene 12b gave compound mono(sulfnyl)dienes 13b with m-chloroperbenzoic acid in CHCl 3 . Compound 15 was synthesized from the reaction of tris(thio)substituted nitrodiene 14 with m-chloroperbenzoic acid in CHCl 3 .
ISSN:1042-6507
1563-5325
DOI:10.1080/713744558