An Efficient Synthesis of 3,4-bis(Tri-n-butylstannyl)furan

Palladium-catalysed addition of hexa-n-butylditin to 2-butyne-1,4-diol, followed by oxidative cyclisation and dehydration gives 3,4-bis(tri-n-butylstannyl)furan in high yield.

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Bibliographic Details
Published in:Synthetic communications 2003-09, Vol.33 (18), p.3205-3209
Main Authors: Mee, Simon P. H., Lee, Victor, Baldwin, Jack E.
Format: Article
Language:English
Subjects:
Acetylene
Furan
Palladium
Stannylation
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Description
Summary:Palladium-catalysed addition of hexa-n-butylditin to 2-butyne-1,4-diol, followed by oxidative cyclisation and dehydration gives 3,4-bis(tri-n-butylstannyl)furan in high yield.
ISSN:0039-7911
1532-2432
DOI:10.1081/SCC-120023442