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Solid-Phase One Step Synthesis of 4H,4′-Exomethylene-bis[quinazolin-2-enols]
The solid-phase one step synthesis of 4H,4′-exomethylene-bis[quinazolin-2-enols] via 1,3-dipolar cycloaddition of urea on benzylideneacetophenone using Sb(III) chloride impregnated alumina is described. The reaction provides 80-85% dimeric quniazolinenols. The process is convenient, cost-effective a...
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Published in: | Synthetic communications 2004-12, Vol.34 (10), p.1819-1823 |
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Main Authors: | , , , |
Format: | Article |
Language: | English |
Subjects: | |
Citations: | Items that this one cites Items that cite this one |
Online Access: | Get full text |
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Summary: | The solid-phase one step synthesis of 4H,4′-exomethylene-bis[quinazolin-2-enols] via 1,3-dipolar cycloaddition of urea on benzylideneacetophenone using Sb(III) chloride impregnated alumina is described. The reaction provides 80-85% dimeric quniazolinenols. The process is convenient, cost-effective and eco-friendly. |
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ISSN: | 0039-7911 1532-2432 |
DOI: | 10.1081/SCC-120034163 |