Implementation of instantaneous comparison methods in temperature gradient evaluation of stirred liquid temperature baths

• Published in: Journal of physics. Conference series 2023-07, Vol.2554 (1), p.12006
• Main Authors: Cheung, Julian C.P., Tsui, C.M., Lam, Brenda H.S., Leung, C.M., Ma, Stanley C.F.
• Format: Article
• Language: English
• Subjects: Calibration; Physics; Resistors; Temperature gradients; Uncertainty
• ISSN: 1742-6588; 1742-6596
• DOI: 10.1088/1742-6596/2554/1/012006

Temperature gradient is an important performance indicator of a stirred liquid bath. Its evaluation requires measuring the temperature differences between different bath positions. A common way to do that is to place two SPRTs at two positions and measure their resistances against a standard resistor ( R SPRT1 / R S and R SPRT2 / R S ) sequentially (the sequential method). A drawback of this method is the existence of a time gap between the two measurements rendering the results susceptible to temporal temperature variation. The instantaneous comparisons method offers a better solution by measuring the resistance ratio of two SPRTs directly ( R SPRT1 / R SPRT2 ) and deriving their temperature difference at the same moment eliminating the time gap. To implement this method at the Standards and Calibration Laboratory (SCL) of Hong Kong, the resistance ratio of SPRT1 to a standard resistor ( R SPRT1 / R s ) is firstly measured to determine the initial bath temperature. After that, the resistance ratios of SPRT1 to SPRT2 ( R SPRT1 / R SPRT2 ) are measured with the two SPRTs placed at different positions and immersion depths in the bath. This paper describes the derivation of the temperature difference from the SPRT resistance ratio using the ITS-90 reference equations and the estimation of the measurement uncertainties. The potential of reducing the uncertainties of measured temperature gradient by leveraging the correlation of the two SPRTs calibrated at the same set of temperature fixed points is discussed. The paper also compares the calibration results obtained by the instantaneous comparisons method and the sequential method.