Validation of a method for the determination of multiclass pesticide residues in fruit juices by liquid chromatography/tandem mass spectrometry after extraction by matrix solid-phase dispersion

A multiresidue method was developed and validated for the determination of pesticide residues (omethoate, dimethoate, carbendazim, propoxur, thiabendazole, carbaryl, pirimicarb, azinphos-methyl, methidathion, and iprodione) in fruit juices. The samples were extracted by matrix solid-phase dispersion...

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Bibliographic Details
Published in:Journal of AOAC International 2002-05, Vol.85 (3), p.724-730
Main Authors: PERRET, Daniela, GENTILI, Alessandra, MARCHESE, Stefano, SERGI, Manuel, D'ASCENZO, Giuseppe
Format: Article
Language:English
Subjects:
Beverages - analysis
Biological and medical sciences
Chromatography, Liquid
Food industries
Food toxicology
Fruit
Fruit and vegetable industries
Fundamental and applied biological sciences. Psychology
Gas Chromatography-Mass Spectrometry
Pesticide Residues - analysis
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Summary:A multiresidue method was developed and validated for the determination of pesticide residues (omethoate, dimethoate, carbendazim, propoxur, thiabendazole, carbaryl, pirimicarb, azinphos-methyl, methidathion, and iprodione) in fruit juices. The samples were extracted by matrix solid-phase dispersion with diatomaceous earth and analyzed by liquid chromatography/tandem mass spectrometry. The method detection limits were
ISSN:1060-3271
1944-7922
DOI:10.1093/jaoac/85.3.724