Basic Aspects in the Application of QCMs as Sensors: A Tutorial

• Published in: IEEE sensors journal 2022-06, Vol.22 (11), p.10163-10172
• Main Authors: Murrieta-Rico, Fabian N., Petranovskii, Vitalii, Galvan, Donald Homero, Antunez-Garcia, Joel, Sergiyenko, Oleg, Lindner, Lars, Rivas-Lopez, Moises, Grishin, Maxim, Sarvadii, Sergey
• Format: Article
• Language: English
• Subjects: Chemical sensors; Frequency measurement; Frequency shift; gas sensors; Loading; Powders; QCM; Quartz crystals; Resonant frequency; Selective adsorption; Sensors; Surface cleaning; Surface topography; Tutorials; Water vapor; Wiring
• ISSN: 1530-437X; 1558-1748
• DOI: 10.1109/JSEN.2022.3148039

Quartz crystal microbalances (QCMs) are devices that have been proven to function as sensors for detecting specific chemical species; this usually requires that the QCM is modified with a material that is capable to interact with the desired compound. Zeolites are an example of materials used as sensitive layer. This due to their capacity for selective adsorption and large surface area; moreover, they can grow directly on the QCM surface. After, the interaction between sensitive layer and analyte, there is a mass change on the QCM surface, which induces a frequency shift in the frequency generated by the QCM. However, the application of QCMs requires that some factors are considered, such as QCM functioning, wiring and surface functionalization. Even when there are commercial devices for QCM operation, a literature revision shows that some concepts are not understood, or some misconceptions are observed. In this work, the basics of QCM are discussed, from principles of operation to an application where a QCM was functionalized to work as sensor for water vapor.